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Nada Perišić-Janjić Institute of Chemistry Faculty of Sciences Trg Dositeja Obradovica 3 21000 Novi Sad Yugoslavia

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Lidija Jevrić Institute of Chemistry Faculty of Sciences Trg Dositeja Obradovica 3 21000 Novi Sad Yugoslavia

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Gordana Bončić-Caričić Faculty of Technology and Metallurgy Kamegijeva 4 11000 Belgrade Yugoslavia

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Bratislav Jovanović Faculty of Technology and Metallurgy Kamegijeva 4 11000 Belgrade Yugoslavia

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The chromatographic behavior of four groups of s -triazine derivatives (15 compounds) has been studied on aminoplast and cellulose thin layers with two mobile phases, methanol-water-acetonitrile, 30 + 20 + X , where X = 1–10 ( v/v ), and methanol-dilute acetic acid, 30 + 20 ( v/v ). The mechanism of retention was investigated by changing of volume fraction of acetonitrile in the first mobile phase. Reversed-phase chromatography occurs on both supports. Retention constants, RMo were determined by extrapolation and good correlation was obtained between retention constants, RMo and log P . These retention constants can be used as the measure of the lipophilicity of compounds. The effect of mobile phase pH on the chromatographic retention of s -triazine derivatives was examined and approximate protonation constants, pKa , were determined on the basis of the dependence of retention on pH. These constants correlated well with Hammett substituent constants σ .

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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