JPC - Journal of Planar Chromatography - Modern TLC
Volume/Issue:
Volume 17: Issue 1
Determination of gallic acid after thin-layer chromatographic and paper chromatographic separations
Authors:
Urszula Hachuła Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Sabina Anikiel Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Marzena Połowniak Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Pages:
51–53
Online Publication Date:
08 Mar 2007
Publication Date:
01 Feb 2004
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jpc.17.2004.1.11
Keywords:
Gallic acid; Separation by TLC and PC; Determination; Pharmaceutical analysis
Restricted access

This paper describes rapid and cost-effective analytical procedures for determination of gallic acid after chromatographic separation. Optimum conditions were established for separation and assay of gallic acid, salicylic acid, and tannic acid by thin-layer and paper chromatography (PC). Detection was by means of a sensitive spectrophotometric method based on the coupled redox-complexation reactions occurring in the system Fe(III), gallic acid, and 2,2′-dipyridyl ( λmax = 522 nm). The procedure was then applied to the determination of gallic acid in a pharmaceutical preparation. Thin layer chromatographic analysis with densitometric UV detection at λ = 280 nm gave comparable results.

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Cover JPC - Journal of Planar Chromatography - Modern TLC
JPC - Journal of Planar Chromatography - Modern TLC
Print ISSN:
0933-4173
Online ISSN:
1789-0993

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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