View More View Less
  • 1 University of Hohenheim Institute of Food Chemistry D-70599 Stuttgart Germany
Restricted access

A new HPTLC method has been established for separation and quantification of six given apolar, fluorescent pyrolytic heterocyclic aromatic amines (HA) of the carboline group. The mobile phase was selected by using a practical and systematic four-level optimization scheme based on the solvent classification system according to Snyder and the PRISMA model of Nyiredy et al. The amines were separated on silica gel 60 F 254 HPTLC plates by a multiple development with diethyl ether. Quantification by fluorescence measurement at λ = 366/>400 nm was performed immediately after development. Limits of detection were in the lownanogram range. The results show that modern planar chromatography is a rapid and cost-efficient alternative method for determination of HA. The method is suitable for both screening and quantification.

  • T. Sugimura , Mutat. Res. 376 (1997) 211–219.

    Sugimura T. , '' (1997 ) 376 Mutat. Res. : 211 -219.

  • M. Bordas, E. Moyano, L. Puignou, and M.T. Galceran , J. Chromatogr. B 802 (2004) 11–17.

    Galceran M.T. , '' (2004 ) 802 J. Chromatogr. B : 11 -17.

  • M. Jaegerstad, A. Laser-Reuterswaerd, R. Oeste, A. Dahlqvist, S. Grivas, K. Olsson, and T. Nyhammar , ACS Symposium Series 215 (The Maillard Reaction in Foods Nutrition), 1983, pp. 507–519.

  • P. Pais and M.G. Knize , J. Chromatogr. B 747 (2000) 139–169.

    Knize M.G. , '' (2000 ) 747 J. Chromatogr. B : 139 -169.

  • S. Knasmüller, M. Murkovic, W. Pfau, and G. Sontag , J. Chromatogr. B 802 (2004) 1–2.

    Sontag G. , '' (2004 ) 802 J. Chromatogr. B : 1 -2.

  • L.R. Snyder , J. Chromatogr. Sci. 16 (1978) 223–234.

    Snyder L.R. , '' (1978 ) 16 J. Chromatogr. Sci. : 223 -234.

  • Sz. Nyiredy, C.A.J. Erdelmeier, B. Meier , and O. Sticher , Planta Med. (1985) 241–246.

For Submission Guideline click HERE

Manuscript Submission: JPC Manuscript Submission

Senior editors

Editor(s)-in-Chief: B. Spangenberg

Managing Editor: Kakuk Ágnes

Editorial Board

  • T.H. Dzido (Lublin, Poland)
  • Á. M. Móricz (Budapest, Hungary)
  • C.F. Poole (Detroit, MI, USA)
  • E. Reich (Muttenz, Switzerland)
  • B. Renger (Radolfzell, Germany)
  • I. Vovk (Ljubljana, Slovenia)

 

Advisory Board

  • E. BODOKI (Cluj-Napoca, Romania)
  • U. A. TH. BRINKMAN (Amsterdam, The Netherlands)
  • I. CHOMA (Lublin, Poland)
  • V. COMAN (Cluj-Napoca, Romania)
  • W. DAMMERTZ (Kressbronn, Germany)
  • K. FERENCZI-FODOR (Budapest, Hungary)
  • G. INDRAYANTO (Surabaya, Indonesia)
  • R. E. KAISER (Bad Dürkheim, Germany)
  • I. KLEBOVICH (Budapest, Hungary)
  • T. KOWALSKA (Katowice, Poland)
  • L. LEPRI (Florence, Italy)
  • E. MINCSOVICS (Budapest, Hungary)
  • D. NUROK (Indianapolis, IN, USA)
  • B. RENGER (Radolfzell, Germany)
  • J. K. RÓŻYŁO (Lublin, Poland)
  • J. SHERMA (Easton, PA, USA)
  • M. WAKSMUNDZKA-HAJNOS (Lublin, Poland)
  • D. WEDGE (Mississippi, USA)

A. Kakuk - Managing Editor, Akadémiai Kiadó
Address: P.O. Box 245. H-1519 Budapest, Hungary
Fax: +36 1 464 82 95
E-mail: jpc@akkrt.hu

Indexing and Abstracting Services:

  • Science Citation Index
  • Sci Search Research Alert
  • Chemistry Citation Index and Current Content/Physical
  • Chemical and Earth Sciences

 

Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Feb 2021 4 0 0
Mar 2021 1 0 0
Apr 2021 1 0 0
May 2021 2 0 0
Jun 2021 1 0 0
Jul 2021 0 0 0
Aug 2021 0 0 0