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  • 1 University of Zagreb Laboratory of Analytical Chemistry, Department of Textile Chemistry and Material Testing, Faculty of Textile Technology Pierottieva 6 10000 Zagreb Croatia
  • | 2 University of Zagreb Horvat, Department of Analytical Chemistry, Faculty of Chemical Engineering and Technology Croatia
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Optimization of the separation and identification of heavy metals present in cotton material has been performed by TLC-densitometry after microwave digestion of cotton samples. The best separation was achieved on precoated microcrystalline cellulose layers with acetonitrile-conc. HCl-water as mobile phase. Optimization of the composition of the ternary mobile phase was achieved by use of experimental design software. Plates were visualized with quercetin-dimethylglyoxime-NH 3 reagent. A highly sensitive CCD color video camera was used to capture the chromatograms under white light.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
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Address
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Springer Nature Switzerland AG
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Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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