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  • 1 Skubiszewski Medical University Department of Pharmacognosy with Medicinal Plant Laboratory 1 Chodżki St. 20-093 Lublin Poland
  • | 2 Technical University Institute of Organic Chemistry, Biochemistry and Biotechnology 27 Wyb. Wyspiańskiego St. 50-370 Wrocław Poland
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Preparative separation and isolation of coumarins from petroleum ether and methanol extracts of the fruits and roots of Peucedanum verticillare L. Koch ex DC ( Umbelliferae = Apiaceae ) have been achieved by column chromatography and normal- and reversed-phase TLC with gradient elution. Isolated coumarins were identified by comparison with standards in analytical TLC and in RP HPLC with gradient elution, by melting point (m.p.) measurement, by UV spectroscopy, by MS, and by 1 H and 13 C NMR spectroscopy. Esculin, umbeliferone, bergapten, xanthotoxin, isoimperatorin, imperatorin, psoralen, and cis -kellactone were isolated for the first time from P. verticillare L. Koch ex DC. Two angular-type pyranocoumarins isolated from the roots and fruits of Peucedanum verticillare L. Koch ex DC. were identified as pteryxin and epoxypteryxin by MS and 1 H and 13 C NMR.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
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1988
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1
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Springer Nature Switzerland AG
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ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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