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  • 1 National Institute of Hydrology Roorkee 247667 India
  • | 2 Indian Institute of Technology Department of Chemistry Roorkee 247667 India
  • | 3 D.A.V. (P.G.) College Department of Chemistry Dehradun 248001 India
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An inexpensive, simple, and reproducible SPE-TLC method has been developed and validated for analysis of haloperidol and its three main metabolites in wastewater. Analysis was performed on C 18 silica gel RPTLC plates with methanol containing 0.001% triethylamine as mobile phase. The development time for 10 cm was 70 min. Detection and quantification were performed by exposing TLC plate to iodine vapor and by UV-visible spectrometry. RF values of haloperidol, metabolite I, metabolite II, and metabolite III were 0.20, 0.05, 0.15, and 0.84 respectively. Recovery of haloperidol and its metabolites from wastewater was in the range 80–90%.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
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Address
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Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
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H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
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ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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