Author:
Irena ChomaM. Curie-Skłodowska University Department of Chromatographic Methods M. Skłodowska Sq. 3 20-031 Lublin Poland

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Fluoroquinolones are a relatively new group of synthetic antibiotics (chemotherapeutics) widely used both in human and animal treatment. Because veterinary enrofloxacin and its main metabolite ciprofloxacin, a widely used human antibiotic, can be present as residues in milk, there is a need for methods for their separation and determination. Matrix solid-phase dispersion (MSPD) on a siliceous sorbent was used for isolation and concentration of enrofloxacin and ciprofloxacin residues from cows’ milk. This preseparation method was combined with high-performance liquid chromatography and with thin-layer chromatography-direct bioautography. Mean recoveries were calculated for different levels of the antibiotics in milk. The results revealed that thin-layer chromatography-direct bioautography can be used for the screening of enrofloxacin and ciprofloxacin at the maximum residue level stipulated for milk by the European Union.

  • J.A. Hernández-Arteseros, J. Barbosa, R. Compaňó , and M.D. Prat , J. Chromatogr. A 945 (2002) 1–24.

    Prat M.D. , '' (2002 ) 945 J. Chromatogr. A : 1 -24 .

  • K.L. Tyczkowska, R.D. Voyksner, L.A. Kevin , and M.G. Papich , J. Chromatogr. B 658 (1994) 341–348.

    Papich M.G. , '' (1994 ) 658 J. Chromatogr. B : 341 -348 .

  • A.L. Cinquina, P. Roberti, L. Giannetti, F. Longo, R. Draisci, A. Fagiolo , and N.R. Brizioli , J. Chromatogr. A 987 (2003) 221–226.

    Brizioli N.R. , '' (2003 ) 987 J. Chromatogr. A : 221 -226 .

  • S.A. Barker , J. Chromatogr. A 880 (2000) 63–68.

    Barker S.A. , '' (2000 ) 880 J. Chromatogr. A : 63 -68 .

  • I.M. Choma and K. Pilorz , J. Liq. Chromatogr. Related Technol. 27 (2004) 2143–2151.

    Pilorz K. , '' (2004 ) 27 J. Liq. Chromatogr. Related Technol. : 2143 -2151 .

  • L. Botz, S. Nagy , and B. Kocsis in: Sz. Nyiredy (Ed.) Planar Chromatography, 1st edn, Springer, Budapest, 2001, pp. 489–516.

    Kocsis B. , '', in Planar Chromatography , (2001 ) -.

  • I.M. Choma, A. Choma, I. Komaniecka, K. Pilorz , and K. Staszczuk , J. Liq. Chromatogr. Related Technol. 27 (2004) 2071–2085.

    Staszczuk K. , '' (2004 ) 27 J. Liq. Chromatogr. Related Technol. : 2071 -2085 .

  • I.M. Choma and I. Komaniecka , J. Liq. Chromatogr. Related Technol. 28 (2005) 2467–2478.

    Komaniecka I. , '' (2005 ) 28 J. Liq. Chromatogr. Related Technol. : 2467 -2478 .

  • T.H. Dzido , J. Planar Chromatogr. 3 (1990) 199–200.

    Dzido T.H. , '' (1990 ) 3 J. Planar Chromatogr. : 199 -200 .

  • I. Choma , J. Liq. Chromatogr. Related Technol. 26 (2003) 2673–2685.

    Choma I. , '' (2003 ) 26 J. Liq. Chromatogr. Related Technol. : 2673 -2685 .

  • K. Pilorz and I. Choma , J. Chromatogr. A 1031 (2004) 303–305.

    Choma I. , '' (2004 ) 1031 J. Chromatogr. A : 303 -305 .

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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