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  • 1 Medical University in Lublin Department of Inorganic Chemistry, Faculty of Pharmacy Staszica 6 St. 20-081 Lublin Poland
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Separation selectivity has been optimized in two-dimensional thin-layer chromatography (2D TLC) by connecting diol or silica plates (on which NP chromatograms were developed) to RP-18W plates (on which reversed-phase chromatograms were developed). Retention of test substances was investigated to select optimum chromatographic systems for separation of selected phenolic compounds by 2D TLC. Selection of optimal mobile phases was performed on the basis of plots of retention against mobile phase composition. The next step of the optimization was calculation of statistical data for correlation of RM values for pairs of chromatographic systems — NP diol-RP C 18 or silica-RP C 18 . Orthogonal chromatographic systems were selected on the basis of these correlations and used to separate phenolic compounds present in plant extracts. For example, extracts from Polygonum sp. and Verbascum sp. were separated by use of optimum 2D TLC systems.

  • J.C. Giddings , Anal. Chem. 56 (1984) 1258A–1260A, 1262A, 1264A, 1268A, 1270A.

    Giddings J.C. , '' (1984 ) 56 Anal. Chem. : 1258A -1260A.

  • J.C. Giddings , J. High Resol. Chromatogr. Chromatogr. Commun. 10 (1987) 319–323.

    Giddings J.C. , '' (1987 ) 10 J. High Resol. Chromatogr. Chromatogr. Commun. : 319 -323.

  • H.J. Cortes , Multidimensional Chromatography Using On-Line Coupled High-Performance Liquid Chromatography and Capillary-Gas Chromatography. In: H.J. Cortes (Ed.) Multidimensional Chromatography, Marcel Dekker, New York, 1990, pp. 251–299.

    Cortes H.J. , '', in Multidimensional Chromatography , (1990 ) -.

  • C.F. Poole, S.K. Poole, W.P.N. Fernando, T.A. Dean, H.D. Ahmed , and J.A. Berndt , J. Planar Chromatogr. 2 (1989) 336–345.+

    Berndt J.A. , '' (1989 ) 2 J. Planar Chromatogr. : 336 -345.

  • G. Guiochon and A.M. Siouffi , J. Chromatogr. 245 (1982) 1–20.

    Siouffi A.M. , '' (1982 ) 245 J. Chromatogr. : 1 -20.

  • G. Guiochon, M.F. Gonnord, A.M. Siouffi , and M. Zakaria , J. Chromatogr. 250 (1982) 1–20.

    Zakaria M. , '' (1982 ) 250 J. Chromatogr. : 1 -20.

  • M. Zakaria, M.F. Gonnord , and G. Guiochon , J. Chromatogr. 271 (1983) 127–192.

    Guiochon G. , '' (1983 ) 271 J. Chromatogr. : 127 -192.

  • G. Guiochon, M.F. Gonnord, M. Zakaria, L.A. Beaver , and A.M. Siouffi , Chromatographia 17 (1983) 121–124.

    Siouffi A.M. , '' (1983 ) 17 Chromatographia : 121 -124.

  • L.A. Beaver and G. Guiochon , USA Patent No. 4469601, 1984.

  • Sz. Nyiredy , Multidimensional Planar Chromatography, LC-GC Eur, Dec 2003.

  • L. Mondello, A.C. Lewis , and K.D. Bartle , Multidimensional Chromatography, Wiley, New York, 2001.

    Bartle K.D. , '', in Multidimensional Chromatography , (2001 ) -.

  • E. Soczewiński, M.A. Hawrył , and A. Hawrył , Chromatographia 54 (2001) 789–794.

    Hawrył A. , '' (2001 ) 54 Chromatographia : 789 -794.

  • M.A. Hawrył and E. Soczewiński , J. Planar Chromatogr. 14 (2001) 415–421.

    Soczewiński E. , '' (2001 ) 14 J. Planar Chromatogr. : 415 -421.

  • M.A. Hawrył, M. Waksmundzka-Hajnos , and T. Inglot , J. Liq. Chromatogr. Related Technol. 28 (2005) 2245–2259.

    Inglot T. , '' (2005 ) 28 J. Liq. Chromatogr. Related Technol. : 2245 -2259.

  • M.A. Hawrył and E. Soczewiński , Chromatographia 52 (2000) 175–178.

    Soczewiński E. , '' (2000 ) 52 Chromatographia : 175 -178.

  • Sz. Nyiredy , Multidimensional Planar Chromatography. In: Planar Chromatography. A Retrospective View for the Third Millennium, Sz. Nyiredy (Ed.) Springer, 2001, 103–119.

  • H. Strzelecka, J. Kamińska, J. Kowalski, E. Walewska , Chemical Methods of Investigations of Plant Materials, PZWL, Warsaw, 1986 (in Polish).

    Walewska E. , '', in Chemical Methods of Investigations of Plant Materials , (1986 ) -.

  • M. Łuczkiewicz, P. Migas, A. Kokotkiewicz, M. Walijewska , and W. Cisowski , J. Planar Chromatogr. 2 (2004) 89–94.

    Cisowski W. , '' (2004 ) 2 J. Planar Chromatogr. : 89 -94.

  • W. Maciejewicz and E. Soczewinski , Chromatographia 51 (2000) 473–477.

    Soczewinski E. , '' (2000 ) 51 Chromatographia : 473 -477.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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