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  • 1 Medical University Department of Pharmaceutical Botany 1 Chodżki Street 20-093 Lublin Poland
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In the 5th European Pharmacopoeia a thin-layer chromatographic (TLC) technique based on analysis of ascorbic acid only is stipulated for qualitative analysis of Rosae pseudofructus, a drug from the dog rose. In this paper a new, simple method is proposed in which the TLC pattern of the flavonoid content is used for effective and reliable quality control of the drug. The method can also be used for identification of different Rosa L. species. The proposed assay uses ultrasound-assisted extraction then clean-up by solid-phase extraction before chromatographic analysis. Quercetin 3-rhamnoside, quercetin 3-glucoside, quercetin 3-rutinoside, catechin, and gallic acid are used as markers. The results reveal that the polyphenol composition of rose pseudo-fruits furnishes a specific TLC chromatogram fingerprint which might be helpful for quality assurance and detection of adulteration of crude extracts.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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