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  • 1 Medical University of Silesia Faculty of Medicine, Department of Chemistry Jordana 19 41-808 Zabrze Poland
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A TLC method with densitometric detection is described for qualitative and quantitative analysis of seven azaarenes — acridine, benzo( h )quinoline, benzo( a )acridine (with benzo( f )quinoline), benzo( c )acridine, dibenzo( a , c )acridine, dibenzo( a , j )acridine (with phenanthridine), and dibenzo( a , h )acridine. The compounds were separated on RP-18/UV plates, in a horizontal chamber, with dichloromethane- n -hexane-2-propanol, 6:4:0.1 ( v / v ), as mobile phase. Quantification of the azaarenes was performed densitometrically by measurement of fluorescence intensity at 380 nm. Limits of determination were from 0.04 to 0.30 ng per spot. The method was used for analysis of the azaarenes in an extract of grilled meat after multistage clean-up based on tandem solid-phase extraction (SPE) on columns packed with Extrelut diatomaceous earth and the cation exchanger propylsulfonic acid (PRS). The concentrations of the benzoacridine and dibenzoacridine isomers were in the range 0.2 to 2.9 ng g −1 meat. The limits of determination in meat were 0.1 ng g −1 for benzo( a )acridine, benzo( c )acridine, dibenzo( a , h )acridine, and dibenzo( a , j )acridine, 0.2 ng g −1 for dibenzo( a , c )acridine, and 0.6 ng g −1 for benzo( h )quinoline.

  • E.A. Bleeker, S. Wiegman, P. de Voogt, M. Kraak, H.A. Leslie, E. de Haas, and W. Admiraal , Rev. Environ. Contam. Toxicol. 173 (2002) 39–83.

    Admiraal W. , '' (2002 ) 173 Rev. Environ. Contam. Toxicol. : 39 -83.

  • D. Warshawsky , Environ. Carcinogenesis Ecotoxicol. Rev. C 10 (1) (1992) 1–71.

    Warshawsky D. , '' (1992 ) 10 Environ. Carcinogenesis Ecotoxicol. Rev. C : 1 -71.

  • I. Sovadinova, L. Blaha, J. Janosek, K. Hilscherova, J.P. Giesy, P.D. Jones, and I. Holoubek , Environ. Toxicol. Chem. 25 (5) (2006) 1291–1297.

    Holoubek I. , '' (2006 ) 25 Environ. Toxicol. Chem. : 1291 -1297.

  • E.A.J. Bleeker, H.G. Van der Geest, H.J. Klamer, P. de Voogt, E. Wind, and M.H. Kraak , Polycyclic Aromat. Compd. 13 (1999) 191–203.

    Kraak M.H. , '' (1999 ) 13 Polycyclic Aromat. Compd. : 191 -203.

  • M. Śkarek, P. Ćupr, K. Reblova, J. Damborsky, B. Marsalek, and I Holoubek , http://www.recetox.muni.cz/coe/sources/workshop_1_rba_pts/VI22-Skarek.pdf

  • S. Kumar, R.L. Chang, A.W. Wood, J.G. Xie, M.T. Huang, X.X. Cui, P.L. Kole, Ch.C. Sikka, S.K. Balani, A.H. Conney, and D.M. Jerina , Carcinogenesis 22 (2001) 951–955.

    Jerina D.M. , '' (2001 ) 22 Carcinogenesis : 951 -955.

  • R.L. Chang, A.W. Wood, S. Kumar, R.E. Lehr, N. Shirai, D.M. Jerina, and A.H. Conney , Carcinogenesis 21 (2000) 1997–2003.

    Conney A.H. , '' (2000 ) 21 Carcinogenesis : 1997 -2003.

  • G. Grimmer , Toxicol. Environ. Chem. 10 (1985) 171–181.

    Grimmer G. , '' (1985 ) 10 Toxicol. Environ. Chem. : 171 -181.

  • H-Y Chen and M. Preston , Anal. Chim. Acta 501 (2004) 71–78.

    Preston M. , '' (2004 ) 501 Anal. Chim. Acta : 71 -78.

  • H-Y Chen and M Preston , Atmos. Environ. 38 (2004) 1023–1028.

    Preston M. , '' (2004 ) 38 Atmos. Environ. : 1023 -1028.

  • L. Warzecha , Chem. Anal. (Warsaw) 38 (1993) 571–583.

    Warzecha L. , '' (1993 ) 38 Chem. Anal. (Warsaw) : 571 -583.

  • I.S. Kozin, O.F. Larsen, P. de Voogt, C. Cooijer, and N.H. Velthorst , Anal. Chim. Acta 354 (1997) 181–187.

    Velthorst N.H. , '' (1997 ) 354 Anal. Chim. Acta : 181 -187.

  • M. Machala, M. Ciganek, L. Blaha, K. Minksova, and J. Vondracek , Environ. Toxicol. Chem. 20 (2001) 2736–2743.

    Vondracek J. , '' (2001 ) 20 Environ. Toxicol. Chem. : 2736 -2743.

  • K. Tyrpień, D. Bodzek, and B. Janoszka , J. Planar Chromatogr. 8 (1995) 75–78.

    Janoszka B. , '' (1995 ) 8 J. Planar Chromatogr. : 75 -78.

  • D. Bodzek, C. Dobosz, B. Janoszka, and J. Konecki , J. Planar Chromatogr. 12 (1999) 265–268.

    Konecki J. , '' (1999 ) 12 J. Planar Chromatogr. : 265 -268.

  • S. Nito and S. Ishizaki , Chemosphere 35 (1997) 1755–1772.

    Ishizaki S. , '' (1997 ) 35 Chemosphere : 1755 -1772.

  • A.A. Herod, M. Millan, T. Morgan, W. Li, J. Feng, and R. Kandiyoti , Eur. J. Mass Spectrom. 11 (2005) 429–442.

    Kandiyoti R. , '' (2005 ) 11 Eur. J. Mass Spectrom. : 429 -442.

  • IARC, Chemical, Environmental and Experimental Data, IARC/WHO Monographs on the Evaluation of Carcinogenic Risks to Humans, 32, Lyon, 1983.

  • A. Sturaro, G. Parvoli, and L. Doretti , Sci. Total Environ. 144 (1994) 285–295.

    Doretti L. , '' (1994 ) 144 Sci. Total Environ. : 285 -295.

  • M.T. Galceran, M.J. Curto, L. Puignou, and E. Moyano , Anal. Chim. Acta 295 (1994) 307–313.

    Moyano E. , '' (1994 ) 295 Anal. Chim. Acta : 307 -313.

  • L. Rivera, M.J. Curto, P. Pais, M.T. Galceran, and L. Puignou , J. Chromatogr. A 731 (1996) 85–94.

    Puignou L. , '' (1996 ) 731 J. Chromatogr. A : 85 -94.

  • W. Koert , Food Eng. Ingredients 28 (4) (2003) 26–28.

    Koert W. , '' (2003 ) 28 Food Eng. Ingredients : 26 -28.

  • G. Grimmer and K.W. Naujack , J. Assoc. Off. Anal. Chem. 69 (1986) 537–541.

    Naujack K.W. , '' (1986 ) 69 J. Assoc. Off. Anal. Chem. : 537 -541.

  • B. Janoszka, L. Warzecha, U. Błaszczyk, and D. Bodzek , Acta Chromatogr. 14 (2004) 129–141.

    Bodzek D. , '' (2004 ) 14 Acta Chromatogr. : 129 -141.

  • B. Janoszka, L. Warzecha, U. Błaszczyk, and D. Bodzek , Acta Chromatogr. 14 (2004) 115–128.

    Bodzek D. , '' (2004 ) 14 Acta Chromatogr. : 115 -128.

  • M. Wilhelm, G. Matuschek, and A. Kettrup , J. Chromatogr. A 878 (2000) 171–181.

    Kettrup A. , '' (2000 ) 878 J. Chromatogr. A : 171 -181.

  • H. Carlsson and C. Osman , J. Chromatogr. A 715 (2000) 31–39.

    Osman C. , '' (2000 ) 715 J. Chromatogr. A : 31 -39.

  • K. Tyrpień and D. Bodzek , J. Planar Chromatogr. 5 (1992) 465–467.

    Bodzek D. , '' (1992 ) 5 J. Planar Chromatogr. : 465 -467.

  • B. Janoszka, D. Bodzek, A. Szotek, and L. Warzecha , J. Planar Chromatogr. 10 (1997) 55–58.

    Warzecha L. , '' (1997 ) 10 J. Planar Chromatogr. : 55 -58.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
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Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
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Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
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Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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