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  • 1 Anhui Agricultural University College of Resources and Environmental Sciences 230036 Hefei Anhui China
  • | 2 Anhui Key Laboratory of Agri-food Safety 230036 Hefei Anhui China
  • | 3 Key Laboratory of Tea Biochemistry and Biotechnology 230036 Hefei Anhui China
  • | 4 International Center for Bamboo and Rattan 100102 Beijing China
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A simple, rapid, and sensitive high-performance thin-layer chromatographic method for analysis of octachlorodipropyl ether (OCDPE) in insecticide formulations has been established and validated. Known amounts of analytical grade OCDPE and its emulsifiable concentrate (EC) or wettable powder (WP) formulations were characterized by HPTLC on silica gel with toluene-acetic acidwater 20:20:1 ( v/v ) as mobile phase; detection was by spraying with silver nitrate-2 m alcoholic potassium hydroxide as chromogenic reagent and exposure to UV light. The plates were evaluated densitometrically at 399 nm. The results indicated that the calibration plot for OCDPE was logarithmic in the range 0.2–5.0 μg per band, and the correlation coefficient for the calibration equation in this range was 0.99. Recoveries from laboratory-prepared test EC and WP formulations using this method were 98.5–103.9% and 95.3–104.3%, respectively, and the respective RSDs were 3.39–4.89% and 2.92–5.33%. The accuracy and precision of the method were suitable for analysis of OCDPE in pesticide formulations.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
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6
Founder Akadémiai Kiadó
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Springer Nature Switzerland AG
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Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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