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  • 1 Medical University of Lublin Department of Inorganic Chemistry Staszica 6 20-081 Lublin Poland
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A strategy has been established for preparative-layer chromatography of the alkaloid fraction from Fumaria officinalis . An extract obtained by maceration and percolation of the milled plant material with 0.5 m aqueous acetic acid was re-dissolved in methanol and fractionated by column chromatography on alumina. Two of the fractions obtained, containing medium polarity alkaloids and strongly polar alkaloids, respectively, were used in the preparative-layer chromatography experiments. Preliminary work focused on investigation of overloading, methods of sampling, effect of layer thickness on band resolution, and the effect of derivatization on the location of separated bands. Another objective of the work was to investigate the use of unidimensional multiple development (UMD) and incremental multiple development (IMD) for resolution of the alkaloids found in Fumaria officinalis extracts.

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  • B. Renger (Radolfzell, Germany)
  • I. Vovk (Ljubljana, Slovenia)

 

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  • R. E. KAISER (Bad Dürkheim, Germany)
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  • E. MINCSOVICS (Budapest, Hungary)
  • D. NUROK (Indianapolis, IN, USA)
  • B. RENGER (Radolfzell, Germany)
  • J. K. RÓŻYŁO (Lublin, Poland)
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  • M. WAKSMUNDZKA-HAJNOS (Lublin, Poland)
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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
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Address
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Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
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Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
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Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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