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  • 1 Medical University of Lublin Faculty of Pharmacy, Chair of Chemistry, Department of Physical Chemistry Staszica 6 20-081 Lublin Poland
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The objective of this study was the use of solid-phase extraction and planar chromatography with diode-array detection for analysis of dyes in beverages. The dyes were chromatographed in normalphase systems on silica, diol, cyanopropyl, and aminopropyl layers and in reversed-phase systems on cyanopropyl, diol, aminopropyl, and octadecyl silica wettable with water. Reversed-phase chromatography was performed with different mobile phase modifiers (tetrahydrofuran, dioxane, methanol, acetonitrile, and acetone) at different concentrations, containing different amines, cationic and anionic ion-pair reagents, buffers, and ammonia, again at different concentrations. On the basis of the results obtained it was possible to choose the best systems for analysis of tartrazine and sunset yellow in beverages. Identification of the analytes was confirmed by the comparison of UV spectra of drink components with those of standards, by use of the diode-array densitometer.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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