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  • 1 Anhui Agricultural University School of Resources and Environment 230036 Hefei, Anhui China
  • | 2 Anhui Key Laboratory of Agri-food Safety 230036 Hefei, Anhui China
  • | 3 International Center for Bamboo and Rattan 100102 Beijing China
  • | 4 Key Laboratory of Bamboo and Rattan Science and Technology 100102 Beijing China
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A high-performance thin-layer chromatographic (HPTLC) method for simultaneous analysis of temephos and fenitrothion in green tea has been established and validated. The sample was extracted with ethyl acetate by mechanical vibration at room temperature and the extract was cleaned by use of an SPE tandem column, before elution with dichloromethane. The extract was applied as bands to glassbacked silica gel 60F254 HPTLC plates. The plates were developed with acetone-hexane 3+7 (v/v), in an unsaturated glass twin-trough chamber. The developed HPTLC plates were evaluated densitometrically. The detection limits of temephos (RF 0.55) and fenitrothion (RF 0.69) were 20 and 10 ng, respectively. Recovery from green tea of the two pesticides at levels of 0.2 to 4 mg kg−1 was 80–107% with relative standard deviations of 4.4–20.2%. The precision and accuracy of the method were generally fit for analysis of temephos and fenitrothion residues in green tea.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
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Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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