JPC - Journal of Planar Chromatography - Modern TLC
Volume/Issue:
Volume 24: Issue 3
Simultaneous NP TLC analysis of the sunscreens diethylamino hydroxybenzoyl hexyl benzoate and octyl methoxycinnamate
Authors:
Anna SobanskaMedical University of Lodz Department of Analytical Chemistry 90-151 Lodz ul. Muszyńskiego 1 Poland

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Elzbieta BrzezinskaMedical University of Lodz Department of Analytical Chemistry 90-151 Lodz ul. Muszyńskiego 1 Poland

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Pages:
227–231
Online Publication Date:
02 Jun 2011
Publication Date:
01 Jun 2011
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jpc.24.2011.3.10
Keywords:
Sunscreen analysis; Diethylamino hydroxybenzoyl hexyl benzoate; Octyl methoxycinnamate; TLC; Spectrodensitometry
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A simple, rapid, and effective method for TLC separation of two EU-authorized UV filters octyl methoxycinnamate (OMC) and diethylamino hydroxybenzoyl hexyl benzoate (DHHB) on silica gel 60 is proposed. Separation conditions were optimized and cyclohexane-diethyl ether-acetone 15:1:2 (ν/ν) was used as mobile phase. Quantification of both filters on the same chromatographic plates was achieved by densitometric scanning in absorption-reflectance mode at 300 and 360 nm, respectively. The method enabled separation of other UV-absorbing ingredients commonly found in cosmetic sunscreen preparations, for example parabens or ethylhexyltriazone (ET). Good quality, linear calibration plots were generated over the range 200–2000 ng per spot both for OMC and DHHB. The method was validated.

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Cover JPC - Journal of Planar Chromatography - Modern TLC
JPC - Journal of Planar Chromatography - Modern TLC
Print ISSN:
0933-4173
Online ISSN:
1789-0993

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Manuscript Submission: HERE

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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