JPC - Journal of Planar Chromatography - Modern TLC
Volume/Issue:
Volume 24: Issue 4
Identification of 11 marker compounds simultaneously in herb Lancea tibetica by using high-performance thin-layer chromatography
Authors:
Zong-Hua Song

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Zhong-Zhi Qian Chinese Pharmacopeia Commission Beijing 100061 China

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Chidananda Rumalla University of Mississippi National Center for Natural Products Research, Research Institute of Pharmaceutical Sciences Oxford MS 38677 USA

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Troy Smillie University of Mississippi National Center for Natural Products Research, Research Institute of Pharmaceutical Sciences Oxford MS 38677 USA

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Ikhlas Khan University of Mississippi, University National Center for Natural Products Research, Research Institute of Pharmaceutical Sciences and Department of Pharmacognosy, School of Pharmacy Oxford MS 38677 USA

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Pages:
312–315
Online Publication Date:
13 Aug 2011
Publication Date:
01 Aug 2011
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jpc.24.2011.4.7
Keywords:
Lancea tibetica ; HPTLC; Identification
Restricted access

A high-performance thin-layer chromatography (HPTLC) method was developed for simple and rapid chemical analysis of Lancea tibetica by using 11 marker compounds. HPTLC was performed on precoated silica 60F254 plates with two mobile phase systems, one was hexanes-ethyl acetate-formic acid 6:3.5:0.5 by volume to identify three furofuranolignans (sylvatesmin, (+)-piperrtol, and horsfieldin), β-sitosterol, and oleanolic acid. The other one was chloroform-methanol-water-formic acid 7:2.5:0.4:0.2 by volume to identify other four furofuranolignans (phillyrin, tibeticoside A, lantibeside C, and lantibeside), verbascoside and isoverbascoside. The developed method was successfully applied for the identification of five L. tibetica samples collected from different regions in China. The developed methods were validated for specificity, stability, repeatability, and robustness.

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Cover JPC - Journal of Planar Chromatography - Modern TLC
JPC - Journal of Planar Chromatography - Modern TLC
Print ISSN:
0933-4173
Online ISSN:
1789-0993

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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