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  • 1 University of Tarbiat Moallem Department of Applied Chemistry, Faculty of Chemistry 49 Mofatteh Avenue Tehran 15614 Iran
  • | 2 Islamic Azad University Chemistry Department, Faculty of Science, Science & Research Branch P. O. Box 14515-775 Poonak-Hesarak, Tehran Iran
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A simple and highly sensitive method is developed for the determination of streptomycin in dosage forms and in biological fluids using ion exchange-high-performance thin-layer chromatography (IE-HPTLC). The method involves the use of titanium(IV) silicate (a synthetic inorganic ion exchanger) coated plates and a mixture of KBr (0.5 m) and ethanol (9:1, ν/ν) as mobile phase. The development time was 18 min. Quantitative measurements were made using a CAMAG TLC Scanner-3 at 359 nm. The streptomycin recovery from the total procedure was equal to 97.9%. The procedure is quantitatively characterized, the linearity was r2 > 0.99, and the relative standard deviation (RSD) was <0.94. The limit of detection (LOD) and limit of quantification (LOQ) were 2.4 and 12 ng, respectively.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
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6
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Springer Nature Switzerland AG
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ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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