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Manuela Stan National Institute for Research and Development of Isotopic and Molecular Technologies 65-103 Donath Street RO-400293 Cluj-Napoca Romania

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Ildikó Lung* National Institute for Research and Development of Isotopic and Molecular Technologies 65-103 Donath Street RO-400293 Cluj-Napoca Romania

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Ocsana Opriş National Institute for Research and Development of Isotopic and Molecular Technologies 65-103 Donath Street RO-400293 Cluj-Napoca Romania

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Maria-Loredana Soran National Institute for Research and Development of Isotopic and Molecular Technologies 65-103 Donath Street RO-400293 Cluj-Napoca Romania

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A high-performance thin-layer chromatography (HPTLC) method has been established for the analysis of α-phellandrene and β-pinene from dill (Anethum graveolens L.) extracts obtained by different extraction techniques and with different solvents and solvent mixtures. The HPTLC analyses were performed in a normal chromatographic chamber on silica gel 60 plates, using petroleum ether-dichloromethane (30:70, v/v) as mobile phase. Photodensitometric evaluation of the chromatographic plates was performed at 600 nm after spraying with vanillin reagent. It was also established that the α-phellandrene and β-pinene extractions depend on the extraction technique and extraction solvent. Taking into account the brief time of extraction and the maximum quantities of α-phellandrene and β-pinene extracted, the most effective method was ultrasound-assisted extraction with n-hexane-diethyl ether (1:1, v/v). Studies of selectivity, linearity, limits of detection and quantification, precision, and accuracy were performed for method validation. The obtained results were compared and correlated with extraction method.

  • S. Heamalatha, S. Swarnalatha, M. Divya, R. Gandhi Lakshmi, A. Ganga Devi, Res. J. Pharm. Biol. Chem. Sci. 2 (2011) 564–574.

    Ganga Devi A , '' (2011 ) 2 Res. J. Pharm. Biol. Chem. Sci. : 564 -574 .

  • T. Ishikaw, M. Kudo, J. Kitajima, Chem. Pharm. Bull. 50 (2002) 501–507.

    Kitajima J , '' (2002 ) 50 Chem. Pharm. Bull. : 501 -507 .

  • V. Radulescu, M.L. Popescu, D.C. Lies, Farmacia 58 (2010) 594–600.

    Lies DC , '' (2010 ) 58 Farmacia : 594 -600 .

  • R. Yazdanparast, S. Baharmikia, Daru 16 (2008) 88–94.

    Baharmikia S , '' (2008 ) 16 Daru : 88 -94 .

  • S. Bahrmika, R. Yazdanparast, Am. J. Chin. Med. 37 (2009) 685–699.

    Yazdanparast R , '' (2009 ) 37 Am. J. Chin. Med. : 685 -699 .

  • H. Hosseinzadeh, G.R. Karimi, M. Ameri, BMC Pharmacol. 2 (2002) 21.

    Ameri M , '' (2002 ) 2 BMC Pharmacol. : 21 -.

  • C. Ma, H. Wang, X. Lu, H. Li, B. Liu, G. Xu, J. Chromatogr. A 1150 (2007) 50–53.

    Xu G , '' (2007 ) 1150 J. Chromatogr. A : 50 -53 .

  • X. Wang, H. Wang, J. Ma, Y. Xu, Y. Guan, Chin. J. Chromatogr. 22 (2004) 101–105.

    Guan Y , '' (2004 ) 22 Chin. J. Chromatogr. : 101 -105 .

  • J.H. Yan, K.W. Tang, M. Zhong, N.H. Deng, Chin. J. Chromatogr. 20 (2002) 569–572.

    Deng NH , '' (2002 ) 20 Chin. J. Chromatogr. : 569 -572 .

  • E. Bramanti, L. D’Ulivo, C. Lomonte, M. Onor, R. Zamboni, G. Raspi, A. D’Ulivo, Anal. Chim. Acta 579 (2006) 38–46.

    D’Ulivo A , '' (2006 ) 579 Anal. Chim. Acta : 38 -46 .

  • M.J. Heravi, H. Sereshti, J. Chromatogr. A 1160 (2007) 81–89.

    Sereshti H , '' (2007 ) 1160 J. Chromatogr. A : 81 -89 .

  • P. Chokeprasert, A. Charles, K.H. Sue, T.C. Huang, J. Food Comp. Anal. 20 (2007) 52–56.

    Huang TC , '' (2007 ) 20 J. Food Comp. Anal. : 52 -56 .

  • M.D. Luque de Castro, L.E. Garcia-Ayuso, Anal. Chim. Acta 369 (1998) 1–10.

    Garcia-Ayuso LE , '' (1998 ) 369 Anal. Chim. Acta : 1 -10 .

  • L. Wang, C.L. Weller, Trends Food Sci. Tech. 17 (2006) 300–312.

    Weller CL , '' (2006 ) 17 Trends Food Sci. Tech. : 300 -312 .

  • C. Liteanu, S. Gocan, T. Hodişan, H. Naşcu, Cromatografia de lichide, Ed. Ştiinţifică, Bucureşti, 1974.

    Naşcu H , '', in Cromatografia de lichide , (1974 ) -.

  • F. Geiss, Fundamentals of Thin Layer Chromatography, Hüthig, Heidelberg, 1987.

    Geiss F , '', in Fundamentals of Thin Layer Chromatography , (1987 ) -.

  • F. Soponar, A.C. Moţ, C. Sârbu, Chromatographia 69 (2009) 151–155.

    Sârbu C , '' (2009 ) 69 Chromatographia : 151 -155 .

  • P.S. Khushboo, V.M. Jadhav, V.J. Kadam, Int. J. PharmTech. Res. 1 (2009) 1122–1128.

    Kadam VJ , '' (2009 ) 1 Int. J. PharmTech. Res. : 1122 -1128 .

  • K. Ferenczi-Fodor, Z. Végh, A. Nagy-Turák, in: Sz. Nyiredy (ed.), Planar Chromatography — A Retrospective View for the Third Millennium, Springer, Budapest, 2001.

  • O. Opriş, V. Coman, F. Copaciu, M. Vlassa, J. Planar Chromatogr. 25 (2012) 516–522.

    Vlassa M , '' (2012 ) 25 J. Planar Chromatogr. : 516 -522 .

  • D.F. Cai, Q. Zhang, J.H. Liu, J. Liq. Chromatogr. Relat. Technol. 34 (2011) 1825–1837.

    Liu JH , '' (2011 ) 34 J. Liq. Chromatogr. Relat. Technol. : 1825 -1837 .

  • B. Fried, J. Sherma, Thin Layer Chromatography, Marcel Dekker Inc., New York, Fourth Edition, Revised and Expanded, Chapter 2, 2005.

    Sherma J , '', in Thin Layer Chromatography , (2005 ) -.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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