Authors:
Qing Zhu

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Haijun Wu

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Fang Wang

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Anqi He Peking University College of Chemistry and Molecular Engineering 100871 Beijing China

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Kun Huang Chinese Academy of Sciences Institute of Process Engineering 100190 Beijing China

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Yongju Wei Hebei Normal University College of Chemistry and Material Science 050024 Shijiazhuang China

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Cuige Liu Hebei Normal University College of Chemistry and Material Science 050024 Shijiazhuang China

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Yanjun Zhai Liaoning University of Traditional Chinese Medicine Dalian College of Pharmacy 116600 Liaoning China

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Shifu Weng Peking University College of Chemistry and Molecular Engineering 100871 Beijing China

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Zhanlan Yang Peking University College of Chemistry and Molecular Engineering 100871 Beijing China

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Yizhuang Xu Peking University College of Chemistry and Molecular Engineering 100871 Beijing China

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Isao Noda University of Delaware Department of Materials Science and Engineering Newark Delaware 19716 United States

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Jinguang Wu Peking University College of Chemistry and Molecular Engineering 100871 Beijing China

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While in situ TLC/FTIR technique has tremendous potential in the analysis of complex mixtures, the conventional stationary phase, such as silica gel, used for TLC/FTIR analysis, has strong absorption in IR region and thus brings about severe interference in the obtained FTIR spectra of the separated samples. In this work, we propose to use lanthanum fluoride fine particles as a new stationary phase of a TLC plate. The average size of LaF3 particles is around 100 nm. FTIR spectrum of the LaF3 particles has no interfering absorption. Preliminary TLC experiments show that mixtures of rhodamine B and methylene blue mixture can be successfully separated by this new TLC plate using LaF3 fine particles as a stationary phase. Methylene blue and rhodamine B from separated spot can be clearly detected by using in situ FTIR spectra.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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