A continuous extraction device for preconcentration of metals with light phase internal recycle has been developed. This system was used for preconcentration of cobalt and uranium from 20–30 dm3 samples with 10.8 dm3/hours feed rate. The emulsion membranes were created of surfactants and LIX 64 N (for cobalt) or di-2ethylhexyl-phosphoric acid (for uranium) as a carrier to control stability and permeability for long time periods. The results from continuous extraction of cobalt and uranium using the device constructed have shown the possibility to reach 100–200-fold preconcentration of metals with high yield (min. 92%).