A conductivity method for combined carbon and free carbon determination in uranium carbide

G. Rizvi; A. De; P. Natarajan

doi:10.1007/bf02162765

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Journal of Radioanalytical and Nuclear Chemistry

Volume/Issue:: Volume 103: Issue 2

A conductivity method for combined carbon and free carbon determination in uranium carbide

Authors:

G. Rizvi

G. Rizvi Bhabha Atomic Research Centre Radiochemistry Division Trombay 400 085 Bombay India

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A. De

A. De Bhabha Atomic Research Centre Radiochemistry Division Trombay 400 085 Bombay India

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P. Natarajan

P. Natarajan Bhabha Atomic Research Centre Radiochemistry Division Trombay 400 085 Bombay India

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Pages:: 95–103

Online Publication Date:: 27 Sep 2005

Publication Date:: 17 Jan 1986

Article Category:: Research Article

DOI:: https://doi.org/10.1007/bf02162765

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Abstract

A conductivity method based on differential temperature oxidation of combined carbon and free carbon has been worked out for their determination in uranium carbide employing purified air for oxidation. The combined carbon determined at 550°C and free carbon at 900°C were found to be 4.58% and 0.27% with a precision of 2% and 11%, respectively. The free carbon determined by the present method and that by dissolution followed by conductivity method agreed within ±5%. Effect of temperature and time on the oxidation of free carbon /taken as graphite/ in air atmosphere was also studied.

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Journal of Radioanalytical and Nuclear Chemistry

Print ISSN:: 0236-5731

Online ISSN:: 1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language	English
Size	A4
Year of Foundation	1968
Volumes per Year	1
Issues per Year	12
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	0236-5731 (Print)
ISSN	1588-2780 (Online)