Authors:
S. Aggarwal Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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R. Duggal Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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H. Jain Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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Abstract  

A method based on the geometric progression decrease of the counts in the far tail of the alpha spectrum is described for the simultaneous determination of plutonium, americium and curium by alpha spectrometry. For evaluating the precision and accuracy, synthetic mixtures were prepared from solutions of enriched isotopes and sources were prepared by direct evaporation method using tetraethylene glycol /TEG/ as a spreading agent and electropolished stainless steel discs as the backing material. Precision and accuracy of about 1% is demonstrated in the determination of244Cm/239Pu,241Am/239Pu,244Cm/233U,241Am/233U and239Pu/233U alpha activity ratios using a 450 mm2 silicon surface barrier detector.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)