Gamma radiolysis of 2-acetylfuran (AF) in 2-propanol, in absence of atmospheric oxygen, has been investigated. The radiation yields of hydrogen, methane at different doses as well as radiolytic products in solution were determined. The radiolytic products were determined by gas chromatography coupled with mass spectrometry. The mechanisms for formation of detected radiolytic products and the effect of (AF) concentration on hydrogen and methane yields are discussed.