Synthesis of 2-dichloromethyl-2-methyl [2-14C]-1,3-dioxolane

I. Jablonkai; F. Dutka

doi:10.1007/bf02218160

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Journal of Radioanalytical and Nuclear Chemistry

Volume/Issue:: Volume 144: Issue 3

Synthesis of 2-dichloromethyl-2-methyl [2-¹⁴C]-1,3-dioxolane

Authors:

I. Jablonkai

I. Jablonkai Hungarian Academy of Sciences Central Research Institute for Chemistry P. O. Box 17 H-1525 Budapest Hungary

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and

F. Dutka

F. Dutka Hungarian Academy of Sciences Central Research Institute for Chemistry P. O. Box 17 H-1525 Budapest Hungary

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Pages:: 173–177

Online Publication Date:: 23 Oct 2005

Publication Date:: 17 Feb 1990

Article Category:: Research Article

DOI:: https://doi.org/10.1007/bf02218160

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Abstract

The labelled compound was prepared by chlorination of [2-¹⁴C]acetone obtained from the barium salt of [1-¹⁴C]acetic acid by pyrolysis. The reaction product 1,1-dichloro [2-¹⁴C]acetone was converted to 2-dichloromethyl-2-methyl [2-¹⁴C]-1,3-dioxolane by condensation with ethylene glycol in the presence of thionyl chloride. Radiochemical yield: 62% based on [1-¹⁴C]acetic acid.

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Journal of Radioanalytical and Nuclear Chemistry

Print ISSN:: 0236-5731

Online ISSN:: 1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language	English
Size	A4
Year of Foundation	1968
Volumes per Year	1
Issues per Year	12
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	0236-5731 (Print)
ISSN	1588-2780 (Online)