Modified pyrohydrolysis apparatus for the separation of fluorine and chlorine trace impurities from nuclear fuel samples for quality control analysis

M. Mahajan; M. Prasad; H. Mhatre; R. Sawant; R. Rastogi; G. Rizvi; N. Chaudhuri

doi:10.1007/bf02060550

Journal of Radioanalytical and Nuclear Chemistry

Volume/Issue:: Volume 148: Issue 1

Modified pyrohydrolysis apparatus for the separation of fluorine and chlorine trace impurities from nuclear fuel samples for quality control analysis

Authors:

M. Mahajan

M. Mahajan Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400085 Bombay (India)

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M. Prasad

M. Prasad Indira Gandhi Centre for Atomic Research Health and Safety Laboratory 603102 Kalpakkam Tamilnadu (India)

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H. Mhatre

H. Mhatre Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400085 Bombay (India)

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R. Sawant

R. Sawant Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400085 Bombay (India)

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R. Rastogi

R. Rastogi Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400085 Bombay (India)

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G. Rizvi

G. Rizvi Bhabha Atomic Research Centre Radiochemistry Division Trombay 400085 Bombay (India)

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N. Chaudhuri

N. Chaudhuri Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400085 Bombay (India)

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Pages:: 93–100

Online Publication Date:: 14 Aug 2005

Publication Date:: 17 Mar 1991

Article Category:: Research Article

DOI:: https://doi.org/10.1007/bf02060550

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Abstract

A quartz pyrohydrolysis apparatus designed for the safe handling of pyrophoric carbide nuclear fuel samples while separating C1 and F trace impurities for quality control analysis is described. It has several advantages over the commonly used pyrohydrolysis apparatus. Performance of the apparatus during routine analysis of a large number of nuclear fuel samples has been found to be quite satisfactory.

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Journal of Radioanalytical and Nuclear Chemistry

Print ISSN:: 0236-5731

Online ISSN:: 1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language	English
Size	A4
Year of Foundation	1968
Volumes per Year	1
Issues per Year	12
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	0236-5731 (Print)
ISSN	1588-2780 (Online)