A titrimetric method for the sequential determination of thorium and plutonium

Keshav Chander; S. Hasilkar; S. Marathe

doi:10.1007/bf02165050

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Journal of Radioanalytical and Nuclear Chemistry

Volume/Issue:: Volume 154: Issue 4

A titrimetric method for the sequential determination of thorium and plutonium

Authors:

Keshav Chander

Keshav Chander Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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S. Hasilkar

S. Hasilkar Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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S. Marathe

S. Marathe Bhabha Atomic Research Centre Fuel Chemistry Division Trombay 400 085 Bombay India

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Pages:: 277–284

Online Publication Date:: 27 Sep 2005

Publication Date:: 17 Jul 1991

Article Category:: Research Article

DOI:: https://doi.org/10.1007/bf02165050

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Abstract

A method for the sequential determination of thorium and plutonium has been developed. In the sample solution containing thorium and plutonium, thorium is first determined by complexometric titration with EDTA and then in the same solution plutonium is determined by redox titration employing potentiometry. Prior to the determination of plutonium, EDTA is destroyed by fuming with concentrated HClO₄. Thorium is determined at 10 mg level and plutonium at 1 mg level with precision and accuracy of better than ±0.5%.

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Journal of Radioanalytical and Nuclear Chemistry

Print ISSN:: 0236-5731

Online ISSN:: 1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language	English
Size	A4
Year of Foundation	1968
Volumes per Year	1
Issues per Year	12
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	0236-5731 (Print)
ISSN	1588-2780 (Online)