Journal of Radioanalytical and Nuclear Chemistry
Volume/Issue:
Volume 175: Issue 6
Preparation and characterization of tris(1, 10-phenanthroline) technetium(III)
Authors: C. Kremer 1 and E. Kremer 1
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  • 1 Facultad de Química Catedra de Química Inorgánica Casilla de Correo 1157 Montevideo Uruguay
DOI:
https://doi.org/10.1007/bf02163748
Page Count:
445–453
Publication Date:
17 Jun 1993
Online Publication Date:
27 Sep 2005
Article Category:
Research Article
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Abstract  

The [Tc(phen)3] (PF6)3 complex has been synthesized by ligand substitution on [Tc(tu)6]3+. The reaction proceeds quickly in aqueous solution. A pure compound is obtained with 40% yield. It was characterized by Tc elemental analysis, cerimetric titration, conductometry and electrophoresis. The corresponding spectroscopic properties (UV, Vis, IR and NMR) are also reported and discussed.

Cover Journal of Radioanalytical and Nuclear Chemistry
Journal of Radioanalytical and Nuclear Chemistry
Print ISSN:
0236-5731
Online ISSN:
1588-2780

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