Author:
Maria Marcilio de Almeida Instituto de Pesquisas Energéticas e Nucleares Comissão Nacional de Energia Nuclear-SP Pinheiros Caixa Postal 11049 05508-900 São Paulo Brasil

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Abstract  

Two simple and selective methods for determination of stannous ion in radiopharmaceutical kits are proposed. One of this permits the estimation of stannic ion. The first method unsed is a potentiometric titration of Sn2+ in HCl medium, using KIO3 solution under nitrogen gas and a platinum redox electrode. The second method consists of a complexometric titration of tin (Sn2+ and Sn4+) using an EDTA standard solution at pH 5.5–5.6 without the use of nitrogen gas. The procedures employed indicate that both methods can be used for routine quantitative determination of tin in most labeled radiopharmaceuticals.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)