Authors:
K. Grant Associated Western Universities Faculty Member from Columbia Basin College Pasco WA (USA)

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R. Lucke Pacific Northwest National Laboratory Advanced Organic Analytical Methods Group 99352 Richland WA (USA)

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S. Clauss Pacific Northwest National Laboratory Advanced Organic Analytical Methods Group 99352 Richland WA (USA)

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G. Mong Pacific Northwest National Laboratory Advanced Organic Analytical Methods Group 99352 Richland WA (USA)

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B. Lerner Pacific Northwest National Laboratory Advanced Organic Analytical Methods Group 99352 Richland WA (USA)

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J. Campbell Pacific Northwest National Laboratory Advanced Organic Analytical Methods Group 99352 Richland WA (USA)

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Abstract  

A technique has been developed for the qualitative determination of low-molecular-weight organic acids in radioactive, mixed hazardous wastes using thermospray liquid chromatography/mass spectrometry. A tank waste was analyzed, and the results indicated the presence of citric, glycolic, acetic, and nitrosoiminodiacetic acid (NIDA). Further investigation revealed NIDA was formed under acidic conditions with the reaction of iminodiacetic acid and the high nitrate/nitrite concentration present in the waste.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)