Journal of Radioanalytical and Nuclear Chemistry
Volume/Issue:
Volume 229: Issue 1-2
Speciation of fission products in raw cow milk by high-performance size exclusion radiochromatography
Authors:
P. Gerhart Comenius University Department of Nuclear Chemistry Mlynská dolina Ch-1 SK-842 15 Bratislava Slovak Republic

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F. Macášek Comenius University Department of Nuclear Chemistry Mlynská dolina Ch-1 SK-842 15 Bratislava Slovak Republic

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P. Rajec Comenius University Department of Nuclear Chemistry Mlynská dolina Ch-1 SK-842 15 Bratislava Slovak Republic

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Pages:
B83–86
Online Publication Date:
12 Apr 2006
Publication Date:
17 Mar 1998
Article Category:
Research Article
DOI:
https://doi.org/10.1007/bf02389451
Restricted access

Abstract  

Speciation of fission products (90Sr,99Tc,137Cs and152Eu) in raw cow milk was studied using the high-performance size exclusion radiochromatography (HP-SERC) by Biosep-SEC-S® column (Phenomenex, USA). The separation fraction were identified by a UV detector (280 nm) and a scintillation radiodetector. The mobile phase was Jenness-Koops buffer that simulated milk serum. Radiocesium was present only in non-protein fractions. The non-protein fractions complexed 17% of technetium and 57% of strontium. About 32% of strontium and 24% of europium were bound on the high molecular weight proteins (micellar casein). Low molecular weight proteins bound about 11% of strontium and 76% of europium. Non-size effects play a dominant role at HPSERC speciation of technetium, 83% of which follow the lightest fractions of milk.

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Cover Journal of Radioanalytical and Nuclear Chemistry
Journal of Radioanalytical and Nuclear Chemistry
Print ISSN:
0236-5731
Online ISSN:
1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation		 1968
Volumes
per Year		 1
Issues
per Year		 12
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)

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