Authors:
A. Dakshinamoorthy Bhabha Atomic Research Centre Kalpakkam Reprocessing Plant Kalpakkam India

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T. Kumar Bhabha Atomic Research Centre Kalpakkam Reprocessing Plant Kalpakkam India

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K. Nandy Bhabha Atomic Research Centre Kalpakkam Reprocessing Plant Kalpakkam India

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R. Iyer Bhabha Atomic Research Centre Kalpakkam Reprocessing Plant Kalpakkam India

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J. Mathur Bhabha Atomic Research Centre, Trombay Radiochemistry Division Mumbai India

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S. Manohar Bhabha Atomic Research Centre, Trombay Radiochemistry Division Mumbai India

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Abstract  

An extraction chromatographic procedure for the recovery of fission product palladium has been developed. The method utilizes Cyanex 471X (tri isobutyl phosphine sulfide, TIPS) impregnated on an inert support, Chromosorb-102. Using this method, quantitative uptake of the metal ion is achieved from nitric acid medium. Thiourea as a suitable stripping agent is suggested. Palladium was estimated spectrophotometrically using Arsenazo III as the chromogenic agent and incorporating a modification in the procedure when the aqueous medium contained thiourea.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)