Authors:
M. Taddei Comissão Nacional de Energia Nuclear, COLAB/CNEN Laboratório de Poços de Caldas CP 913 37701-970 Poços de Caldas, MG Brazil

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N. Silva

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E. Fernandes Universidade de São Paulo, CENA/USP Centro de Energia Nuclear na Agricultura CP 96 13400-970 Piracicaba, SP Brazil

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M. Cipriani Comissão Nacional de Energia Nuclear, COLAB/CNEN Laboratório de Poços de Caldas CP 913 37701-970 Poços de Caldas, MG Brazil

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Abstract  

A radiochemical procedure for the determination of alpha-emitting isotopes of uranium and thorium in vegetables and excreta has been optimized, involving sample dissolution, separation by ionic exchange resin, electrodeposition and alpha-spectroscopy. Uranium and thorium isotopes were determined separately to prevent interference of 228Th from 232U tracer with 228Th from natural series of 232Th. This procedure was applied to faeces from people living in the Poços de Caldas plateau, a high natural radioactivity region of Brazil, and vegetables from the Laboratory of Environmental Monitoring (EML/DOE). Results show a chemical recovery of 80–95% for uranium and 46–72% for thorium.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)