Author:
A.A. Oladipo Obafemi Awolowo University Centre for Energy Research and Development Ile-Ife Nigeria

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Abstract  

The precision obtainable by instrumental neutron activation analysisdepends strongly on the quality of the calibration of the gamma-ray spectrometerused for measuring the irradiated samples. Even when relative standardizationis employed, practical experience has shown the importance of detector calibration.This is especially relevant when radionuclides of varying activities are involved.The problems often encountered are those of intolerable high dead time andthe occurrence of summed peaks in the gamma-ray spectra. A simple but accuratesemi-empirical formula is presented that could effectively predict the efficiencyof a detector at any source-to-detector distance. Experimental data obtainedat 0, 50, 100, 200 mm source-to-detector distances are used to demonstratethe usefulness of this formulation. In addition, nine elements were analyzedin the NIST Orchard Leaves using absolute standardization including four elementsSm, Ta, Au, and La for which no certified values could be obtained.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)