Authors:
J. Gascón Centro de Investigaciones Energéticas Medioambientales y Tecnológicas (CIEMAT) Proyecto Reelaboración Hidrometalúrgica y Residuos Radiactivos, Departamento de Fisión Nuclear Edificio 18, CIEMAT Avda. Complutense, n° 22 28040 Madrid Spain

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A. Muñoz Centro de Investigaciones Energéticas Medioambientales y Tecnológicas (CIEMAT) Avda. Complutense, n° 22 28040 Madrid Spain

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Abstract  

In radiochemical analysis, specially by using high resolution alpha-spectrometry, a key issue is the determination of the radiochemical yield. Radiochemical yield allows to determine the concentration of the radionuclide of interest and the quality of the chemical separation. To determine the radiochemical yield it is necessary to know the solid state detector efficiency, which can be obtained by calibration with a circular calibrated source. In this paper the optimization of the parameters affecting both the calibration and measurement of a source by alpha-spectrometry is described. The optimization is based on two sets of data: experimental and theoretical. Experimental data were obtained from the calibration of the solid state detector with four calibrated 241Am sources. Theoretical data were calculated by geometry formulas and were verified experimentally.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)