Authors:
F. De Corte Laboratory of Analytical Chemistry, Institute for Nuclear Sciences, Ghent University Proeftuinstraat 86, B-9000 Gent, Belgium

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M. Dejaeger Laboratory of Analytical Chemistry, Institute for Nuclear Sciences, Ghent University Proeftuinstraat 86, B-9000 Gent, Belgium

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S. M. Hossain Laboratory of Analytical Chemistry, Institute for Nuclear Sciences, Ghent University Proeftuinstraat 86, B-9000 Gent, Belgium

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D. Vandenberghe Laboratory of Analytical Chemistry, Institute for Nuclear Sciences, Ghent University Proeftuinstraat 86, B-9000 Gent, Belgium

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A. De Wispelaere Laboratory of Analytical Chemistry, Institute for Nuclear Sciences, Ghent University Proeftuinstraat 86, B-9000 Gent, Belgium

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P. Van den Haute Laboratory for Mineralogy, Petrography and Micropedology, Geological Institute, Ghent University Krijgslaan 281, B-9000 Gent, Belgium

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Summary  

Recently, in our laboratory an intercomparison was made of methods for the annual radiation dose determination (assessed from direct radiation counting and/or from the measurement of the K, Th and U contents) applied to luminescence dating of loess and sand sediment, whereby the emphasis was put on their precision and accuracy. Although these properties are important, the duration of the measurement is also a practically relevant aspect. Indeed, direct alpha, beta and gamma-counting can last a week or more, and the determination of K, Th and U via NAA can take up to three weeks to enable proper gamma-ray spectrometry of the long-lived 233 Th/233Pa. Therefore, in the present work the performance of k0-based epiCd-NAA (ENAA, with irradiation under a cadmium cover) when applied to sediments is compared to k0-NAA. As concluded, with the use of k0-ENAA the analysis turnaround time could be considerably reduced from ~3 weeks to ~ 2.5days, while maintaining satisfactory accuracy, precision and determination sensitivity.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)