A recent study has indicated the feasibility of recycling of chemicals from alkaline waste generated in the preparation of
UO3 microspheres by the internal gelation process. Present paper investigates the recycle process, the volume of the secondary
uranium waste. Result shows that prior to start the recycle process, the waste solution should be freed from uranium by ion-exchange.
Optimized experimental condition to achieve maximum reduction in the volume of uranium based waste is discussed.