Authors:
R. Shabana Atomic Energy Establishment Nuclear Chemistry Department Cairo (Egypt)

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F. Hafez Atomic Energy Establishment Nuclear Chemistry Department Cairo (Egypt)

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Abstract  

The effect of TBP as well as the organic diluents on the polarographic wave of U(VI) reduction has been investigated in sulphuric and perchloric acids. It was found that the presence of TBP traces in the solution to be analyzed induced another wave which was more prominent in sulphuric acid solutions. This can be eliminated by boiling the solutions for about 5 min before their analysis for uranium. The effect of supporting electrolyte on the polarographic reduction of U(VI) was also studied and the use of 6N HClO4 was recommended.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)