Challenges and successes in the use of neutron activation analysis procedures for value assignment of animal serum and bovine liver Standard Reference Materials

R. Zeisler; R. Greenberg; E. Mackey; K. Murphy; R. Spatz; B. Tomlin

doi:10.1007/s10967-009-0089-4

Journal of Radioanalytical and Nuclear Chemistry

Volume/Issue:: Volume 281: Issue 1

Challenges and successes in the use of neutron activation analysis procedures for value assignment of animal serum and bovine liver Standard Reference Materials

Authors:

R. Zeisler

R. Zeisler National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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R. Greenberg

R. Greenberg National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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E. Mackey

E. Mackey National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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K. Murphy

K. Murphy National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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R. Spatz

R. Spatz National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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, and

B. Tomlin

B. Tomlin National Institute of Standards and Technology Analytical Chemistry Division 100 Bureau Dr Gaithersburg MD 20899-8395 USA

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Pages:: 11–15

Online Publication Date:: 12 Jun 2009

Publication Date:: 01 Jul 2009

Article Category:: Research Article

DOI:: https://doi.org/10.1007/s10967-009-0089-4

Keywords:: Chemical separation; Radiochemistry; Gamma-ray spectrometry; Low level trace elements

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Abstract

Analyses for value assignment in the renewal Standard Reference Materials^® SRM 1598a Animal Serum and SRM 1577c Bovine Liver included extensive characterization by neutron activation analysis (NAA). Conventional instrumental NAA procedures were complemented by pre-irradiation chemical separations for the determination of Al, V, Mn, and Cu, radiochemical separations for the determination of Ag, As, Cd, Cr, Cu, Mo, Sb, and Se, and the use of (anti-) coincidence gamma-ray spectrometry systems for the instrumental determination of Ag, Cr, and Hg. The previous materials, SRMs 1598, 1577, and 1577b, were analyzed together with the new materials for quality control.

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Journal of Radioanalytical and Nuclear Chemistry

Print ISSN:: 0236-5731

Online ISSN:: 1588-2780

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Journal of Radionalytical and Nuclear Chemistry
Language	English
Size	A4
Year of Foundation	1968
Volumes per Year	1
Issues per Year	12
Founder	Akadémiai Kiadó
Founder's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher	Akadémiai Kiadó Springer Nature Switzerland AG
Publisher's Address	H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible Publisher	Chief Executive Officer, Akadémiai Kiadó
ISSN	0236-5731 (Print)
ISSN	1588-2780 (Online)