Neutron activation analysis was used to investigate and quantify the level of heavy metal uptake in the marine environment of Lake Austin in Austin, TX. Specifically, the samples studied were largemouth bass, or micropterus salmoides. The presence of heavy metals in the food chain presents multiple hazards, mostly as a food hazard for those species that ingest the fish, namely humans. To measure the concentrations of heavy metals in various fish samples, the nuclear analytical technique of neutron activation analysis (NAA) was used. Both epithermal and thermal irradiations were conducted for the NAA to look for short and long-lived radioisotopes, respectively. The samples themselves consisted of liver and tissue samples for each of the fish caught. Each sample was freeze-dried and homogenized before irradiation and spectrum acquisition. The results showed that all levels of heavy metals were not sufficient enough to make the fish unsafe for eating, with the highest levels being found for iron and zinc. Gold was found to be at much higher concentrations in the younger fish and virtually non-existent in the larger of the samples.