Author:
S. Behrendt Carleton University Department of Chemistry Ottawa Canada

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Abstract  

For the positional isotopic analysis of tritium-labelled organic compounds which are isolated at the end of a tracer experiment, it is proposed to render high-resolution triton-NMR spectroscopy sufficiently sensitive as follows. Andrew's rotating magnetic field is used to narrow the NMR lines that are detected by observing the anisotropy of the β-radiation of the sample which is kept at 0.01 °K by a helium-dilution refrigerator. In this context, the usefulness of the rotating magnetic field for cryogenic proton-NMR spectroscopy is pointed out.

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
1
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)