Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 100: Issue 2
Identification of acrylate copolymers using pyrolysis and gas chromatography
Authors:
Zbigniew CzechWest Pomeranian University of Technology Institute of Chemical Organic Technology Pułaskiego 10 70-322 Szczecin Poland

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Robert PełechWest Pomeranian University of Technology Institute of Chemical Organic Technology Pułaskiego 10 70-322 Szczecin Poland

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Pages:
641–644
Online Publication Date:
19 Jun 2009
Publication Date:
01 May 2010
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-009-0142-0
Keywords:
Acrylic and methacrylic copolymers; Pyrolysis; Thermal degradation products; Analysis and identification
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Abstract  

A combination of pyrolysis and gas chromatography were used to investigate thermal degradation products formed from acrylic copolymers containing alkyl acrylate and methacrylate. The method provided an analytical tool for characterizing the chemical composition and structure of the degradation products. Thermal degradation of the synthesized copolymers was analyzed using isothermal (250 °C) pyrolysis–gas chromatography. The degradation process, and the nature and amount of pyrolysis products, provides relevant information about the thermal degradation of acrylic copolymers and the mechanism of pyrolysis. During pyrolysis, the formation of corresponding olefins, alcohols, acrylates and methacrylate was observed.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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