Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 101: Issue 3
X-ray, SEM, and DSC studies of ferroelectric Pb1−XBaXTiO3 ceramics
Authors:
M. Roy Department of Physics, M. L. Sukhadia University, Udaipur, 313002 Rajasthan India

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Praniti Dave Department of Physics, M. L. Sukhadia University, Udaipur, 313002 Rajasthan India

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Shiv Barbar Department of Physics, M. L. Sukhadia University, Udaipur, 313002 Rajasthan India

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Sumit Jangid Department of Physics, M. L. Sukhadia University, Udaipur, 313002 Rajasthan India

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D. Phase UGC-DAE-CSR, Indore, India

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A. Awasthi UGC-DAE-CSR, Indore, India

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Pages:
833–837
Online Publication Date:
18 Sep 2009
Publication Date:
01 Sep 2010
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-009-0422-8
Keywords:
Ferroelectrics; Heat capacity; Phase transition; SEM; X-ray diffraction
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Abstract  

The polycrystalline ferroelectric compounds of general formula Pb1−XBaXTiO3 with X = 0.00, 0.1, 0.2 and 0.5 were prepared by high temperature solid-state reaction technique using high purity oxides and carbonates. The compounds formation was confirmed by X-ray diffraction and all the X-ray peaks were indexed with tetragonal structure of space group P4mm. Morphology and particle size of the compounds were obtained using scanning electron microscopy. Ferroelectric phase transition, enthalpy change, and specific heat of the compounds were obtained using modulated differential scanning calorimetry. It was observed that the phase transition temperature decreased linearly with the increase of substitution concentration.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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