Geopolymers
Inorganic polymeric new materials
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Chun-Hong Jiang
Chun-Hong Jiang
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Li-Fang Song
Li-Fang Song
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Cheng-Li Jiao
Cheng-Li Jiao
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Graduate School of the Chinese Academy of Sciences, Beijing 100049, People's Republic of China
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Jian Zhang
Jian Zhang
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
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Li-Xian Sun
Li-Xian Sun
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
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Fen Xu
Fen Xu
Faculty of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, People's Republic of China
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Huan-Zhi Zhang
Huan-Zhi Zhang
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
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Qing-Yang Xu
Qing-Yang Xu
Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian 116023, People's Republic of China
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Zelimir Gabelica
Zelimir Gabelica
Université de Haute Alsace, ENSCMu, Lab. LPI-GSEC, 3, Rue A. Werner, 68094, Mulhouse Cedex, France
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Abstract
Two metal-organic frameworks, Ca(2,6-NDC)(DMF) (1) and Mn3(2,6-NDC)3(DMF)4 (2) (where 2,6-NDC = 2,6-naphthalene dicarboxylate and DMF = N,N′-dimethylformamide) have been solvothermally synthesized under optimized conditions and characterized by X-ray powder diffraction, elemental analysis, FT-IR spectroscopy, and TG analysis. The thermal decomposition characteristics were investigated under air atmosphere from 300 to 1,170 K (for 1) and from 300 to 971 K (for 2). The molar heat capacities were measured from 198 to 548 K (for 1) and from 198 to 448 K (for 2) by temperature modulated differential scanning calorimetry (TMDSC) for the first time. The fundamental thermodynamic parameters such as entropy and enthalpy variations with temperature were calculated based on the experimentally determined molar heat capacities.
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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