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J. A. Stratis Laboratory of Analytical Chemistry, Department of Chemistry, Faculty of Sciences, Aristotle University, 54 124, Thessaloniki, Greece

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M. Lalia-Kantouri Laboratory of Inorganic Chemistry, Department of Chemistry, Aristotle University, P. O. Box 135, 54 124, Thessaloniki, Greece

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El. Charalambous Department of Antiquities, Nicosia, Republic of Cyprus

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A. Charalambous Laboratory of Analytical Chemistry, Department of Chemistry, Faculty of Sciences, Aristotle University, 54 124, Thessaloniki, Greece

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N. Kantiranis Department of Mineralogy-Petrology-Economic Geology, Faculty of Sciences, Aristotle University, 54 124, Thessaloniki, Greece

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Abstract

This study is focused on simultaneous thermoanalytical investigations by TG/DTG-DTA technique applied for characterization of samples collected from archaeological site of Nicosia, Cyprus, dating to seventeenth century and gave new information on the firing technology. The ceramic samples derived from Ottomanic tobacco pipes were characterized by the related techniques such as X-ray powder diffraction for the mineralogical composition, and inductively coupled plasma-atomic emission spectrometry and micro-X-ray fluorescence spectroscopic analysis for the chemical content. It was found that they consisted mainly of quartz, calcite, feldspars, and micas. For the majority of the investigated ceramic samples, the thermal behavior investigation collaborates with their mineralogical findings, and resulted to the firing temperature at ~700 °C, due to the existence of calcite. Only in two samples with very high content in quartz, absence of calcite, low amounts of adsorbed water and of total mass loss, and absence of micas, the firing process resulted up to 1000 °C.

  • 1. Feliu, MJ, Edreira, MC, Martín, J. Application of physical–chemical analytical techniques in the study of ancient ceramics. Anal Chim Acta 2004 502:241250 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 2. Bertolino, SR, Fabra, M. Provenance and ceramic technology of pot sherds from ancient Andean cultures at the Ambato valley, Argentina. Appl Clay Sci 2003 24:2134 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 3. Bagnasco, MB, Casoli, A, Chiari, G, Compagnoni, R, Davit, P, Mirti, P. Mineralogical and chemical composition of transport amphorae excavated at Locri Epizephiri (southern Italy). J Cult Herit 2001 2:229239 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 4. Odlyha, M Thermal analysis 2000 E Ciliberto G Spoto eds. Modern analytical methods in art and archeology Wiley Interscience New York 279320.

    • Search Google Scholar
    • Export Citation
  • 5. Robinson, R. Tobacco pipes of Corinth and of the Athenian Agora. Hesperia. 1985;54:149203 .

  • 6. Uzi, B. Clay tobacco pipes and coffee cup sherds in the archaeology of the middle east: artifacts of social tensions from the Ottoman past. Int J Hist Archaeol. 1999;3 /3 137151.

    • Search Google Scholar
    • Export Citation
  • 7. Shoval, S, Michaelian, KH, Boudeulle, M, Panczer, G, Lapides, I, Yariv, S. Study of thermally treated dickite by infrared and micro-Raman spectroscopy using curve-fitting technique. J Therm Anal Cal 2002 69:205225 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 8. Shoval, S, Gaft, M, Panczer, G. Luminescence of Cr3+ in natural and calcined diaspore. J Therm Anal Cal 2003 71:699706 .

  • 9. Daszkiewicz, M, Raabe, J Technology of firing of grey ware so called “Siwak” from Late Medieval Plock 1995 P Vincenzini eds. The ceramics cultural heritage Techna: Monographs in Materials and Society 2 Faenza 349359.

    • Search Google Scholar
    • Export Citation
  • 10. Moropoulou, A, Bakolas, A, Bisbikou, K. Characterization of ancient, byzantine and later historic mortars by thermal and X-ray diffraction techniques. Thermochim Acta 1995 269 /270 779795 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 11. Campanella, L, Favero, G, Flamini, P, Tomassetti, M. Prehistoric terracottas from the Libyan tadrart acacus. Thermoanalytical study and characterization. J Therm Anal Cal 2003 73:127142 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 12. Drebushchak, VA, Mylnikova, LN, Drebushchak, TN, Boldyrev, VV. The investigation of ancient pottery. Application of thermal analysis. J Therm Anal Cal 2005 82:617626 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 13. Papadopoulou, DN, Lalia-Kantouri, M, Kantiranis, N, Stratis, JA. Mineralogical contribution to the ancient ceramics and natural clay characterization. J Therm Anal Cal 2006 84:3945 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 14. Bruno, P, Caselli, M, Curri, ML, Genga, A, Striccoli, R, Traini, A. Chemical characterisation of ancient pottery from south of Italy by inductively coupled plasma atomic emission spectroscopy (ICP-AES), statistical multivariate analysis of data. Anal Chim Acta 2000 410:193202 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 15. Zhu, J, Shan, J, Qiu, P, Qin, Y, Wang, C, He, D, Sun, B, Tong, P, Wu, S. The multivariate statistical analysis and XRD analysis of pottery at Xigongqiao site. J Archaeol Sci 2004 31:16851691 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 16. Ion, R-M, Ion, M-L, Fierascu, RC, Serban, S, Dumitiu, I, Radivici, C, Bauman, I, Cosulet, S, Niculescu, VIR. Thermal analysis of Romanian ancient ceramics. J Therm Anal Cal 2010 102:393398 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 17. Albarez, JI, Navarro, I, Garcia Casado, PJ. Thermal, mineralogical and chemical studies of the mortars used in the cathedral of Pamplona (Spain). Thermochim Acta 2000 365:177187 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 18. Iordanidis, A, Garcia-Guinea, J, Strati, A, Gkiourtzina, A, Papoulidou, A. Thermal, mineralogical and spectroscopic study of plasters from three post-Byzantine churches from Kastoria (northern Greece). J Therm Anal Cal 2010 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 19. Papadopoulou, D, Zachariadis, G, Anthemidis, A, Tsirliganis, N, Stratis, JA. Microwave-assisted versus conventional decomposition procedures applied to a ceramic potsherd standard reference material by inductively coupled plasma atomic emission spectrometry. Anal Chim Acta 2004 505:173181 .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 20. Webb, TL, Kruger, JE Carbonates 1970 RC Mackenzie eds. Differential thermal analysis Academic Press London 303341.

  • 21. Greenwood, NN, Earnshaw, A Chemistry of the elements 1984 Pergamon Oxford.

  • 22. Lopez-Arce, P, Garcia-Guinea, J, Gracia, M, Obis, J. Bricks in historical buildings of Toledo City: characterisation and restoration. Mater Charact 2003 50:5968 .

    • Crossref
    • Search Google Scholar
    • Export Citation
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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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