Geopolymers
Inorganic polymeric new materials
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D. V. Pinakov
D. V. Pinakov
Nikolaev Institute of Inorganic Chemistry, Siberian Branch of Russian Academy of Sciences, Ac. Lavrentyev Ave. 3, Novosibirsk-90 630090, Russia
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V. A. Logvinenko
V. A. Logvinenko
Nikolaev Institute of Inorganic Chemistry, Siberian Branch of Russian Academy of Sciences, Ac. Lavrentyev Ave. 3, Novosibirsk-90 630090, Russia
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G. N. Chekhova
G. N. Chekhova
Nikolaev Institute of Inorganic Chemistry, Siberian Branch of Russian Academy of Sciences, Ac. Lavrentyev Ave. 3, Novosibirsk-90 630090, Russia
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Yu. V. Shubin
Yu. V. Shubin
Nikolaev Institute of Inorganic Chemistry, Siberian Branch of Russian Academy of Sciences, Ac. Lavrentyev Ave. 3, Novosibirsk-90 630090, Russia
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Abstract
Inclusion compounds (intercalates) of fluorinated graphite matrix with acetone (C2FxBrz·y(CH3)2CO, x = 0.49, 0.69, 0.87, 0.92, z ≈ 0.01) were prepared by guest substitution from acetonitrile to acetone. The kinetics of the thermal decomposition (the first stage of filling → the second stage of filling) was studied under isothermal conditions at 292–313 K. The relationship of the host matrices structure with inclusion compounds thermal properties and kinetic parameters is discussed.
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1. Pinakov, DV, Logvinenko, VA 2006 The relationship between properties of fluorinated graphite intercalates and matrix composition. 1. Intercalates with acetonitrile. J Therm Anal Calorim 86:173–178 .
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2. Pinakov, DV, Logvinenko, VA, Shubin, YuV, Chekhova, GN 2007 The relationship between properties of fluorinated graphite intercalates and matrix composition. 2. Intercalates with chloroform. J Therm Anal Calorim 90:399–405 .
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3. Pinakov, DV, Logvinenko, VA, Shubin, YuV, Chekhova, GN 2009 Relationship between properties of fluorinated graphite intercalates and matrix composition. Part III. Intercalates with 1,2-dichloroethane. J Therm Anal Calorim 96:501–505 .
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4. Pinakov, DV, Logvinenko, VA, Shubin, YuV, Chekhova, GN 2010 The relationship between properties of fluorinated graphite intercalates and matrix composition. Part 4. Intercalates with methylene dichloride. J Therm Anal Calorim 100:163–169 .
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8. Chekhova, GN, Ukraintseva, EA, Ivanov, IM, Yudanov, NF, Shubin, YuV, Logvinenko, VA, Pinakov, DV, Fadeeva, VP, Alferova, NI 2005 Influence of the matrix composition on the properties of fluorinated graphite inclusion compounds with acetonitrile. J Inorg Chem 50 7 1055–1061.
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9. Shubin, YuV, Pinakov, DV, Chekhova, GN, Alferova, NI, Logvinenko, VA 2006 Phase transitions of intercalation inclusion compounds C2F0.92Br0.01 yCH3CN in the temperature range 20–260 °C. J Struct Chem 47:1141–1154 .
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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