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Preeti Gupta
Preeti Gupta
Department of Chemistry, D. D. U. Gorakhpur University, Gorakhpur 273009, India
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Tanvi Agrawal
Tanvi Agrawal
Department of Chemistry, U.P. Autonomous College, Varanasi, India
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S. S. Das
S. S. Das
Department of Chemistry, D. D. U. Gorakhpur University, Gorakhpur 273009, India
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N. B. Singh
N. B. Singh
Research and Technology Development Centre, School of Engineering and Technology, Sharda University, Greater Noida, India
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Abstract
Reactions of nitrophenols have been studied in the eutectic melt of 8-hydroxyquinoline–benzoic acid, where it reacted with 8-hydroxyquinoline. The reactions were also carried out in solution. The reaction products obtained from both the methods were characterized by FT-IR, differential scanning calorimetry, X-ray diffraction technique and microstructural investigations. The reaction products obtained from eutectic melt were analyzed for C, H, N. The results showed that reaction products obtained from both the methods are same. An attempt has been made to propose the overall mechanism of the reaction in the eutectic melt.
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1. Feng, X, Shi, L, Wang, S, Ma, S 2008 Effect of NaNO3–KNO3 eutectic in fabricating ZnO nanocrystals. Solid State Ionics 179:2077–2079 .
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2. Singh, NB, Ojha, AK 2001 Preparation of NiO through NaNO3–KNO3 eutectic melt and its catalytic activity during the decomposition of polystyrene. Thermochim Acta 378:87–96 .
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3. Wang, YG, Ma, JF, Tao, JT, Zhu, XY, Zhou, J, Zhao, ZQ, Xie, LJ, Tian, H 2006 Morphology-controlled synthesis of CdWO4 nanorods and nanoparticles via a molten salt method. Mater Sci Eng B 130:277–281 .
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4. Singh, NB, Ojha, AK 2002 Formation of copper oxide through NaNO3–KNO3 eutectic melt and its catalytic activity in the decomposition of ammonium perchlorate. Thermochim Acta 390:67–72 .
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17. Singh, NB, Das, SS, Singh, NP, Agrawal, T 2008 Computer simulation, thermodynamics and microstructural studies of benzamide–benzoic acid eutectic system. J Cryst Growth 310:2878–2884 .
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
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| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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