Authors:
B. A. Howell Department of Chemistry and Center for Applications in Polymer Science, Central Michigan University, Mt. Pleasant, MI, 48859-0001, USA

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H. Dangalle Department of Chemistry and Center for Applications in Polymer Science, Central Michigan University, Mt. Pleasant, MI, 48859-0001, USA

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M. Al-Omari Department of Chemistry and Center for Applications in Polymer Science, Central Michigan University, Mt. Pleasant, MI, 48859-0001, USA

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Abstract

A difunctional imide monomer may be produced from 4-nitrophthalic anhydride and m-phenylenediamine. The requisite anhydride may be generated by nitration of phthalimide followed by hydrolysis to the corresponding acid and dehydration. All intermediate compounds have been fully characterized using spectroscopic and thermal methods.

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  • 2. Borup, R, Meyers, J, Pivovar, B, Kim, YS, Mukundan, R, Garland, N, Myers, D, Wilson, M, Garzon, F, Wood, D, Zelenay, P, More, K, Stroh, K, Zawodzinski, T, Boncella, J, McGrath, JE, Inaba, M, Miyatake, K, Hori, M, Ota, K, Ogumi, Z, Miyata, S, Nishikata, A, Siroma, Z, Iwashita, Y. Scientific aspects of polymer electrolyte fuel cell durability and degradation. Chem Rev. 2007;107:39043951. .

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  • 3. Papadimitriou, KD, Andreopoulou, AK, Kallitsis, JK. Phosphonated fully aromatic polyethers for PEMFCs applications. J Polym Sci A. 2010;48:28172827. references cited therein.

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  • 4. Lafitte B , Jannasch P. On the prospects for phosphonated polymers as proton-exchange fuel cell membranes. Advances in fuel cells, Chapter 3. Oxford: Elsevier Ltd.; 2007. p. 11985.

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  • 5. Huntress, EH, Shriner, RL. 4-Nitrophthalimide. Org Synth. 1936;16:58.

  • 6. Huntress, EH, EL Shloss Jr, Ehrlich, P. 4-Nitrophthalic acid. Org Synth. 1936;16:56.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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