Authors:
O. S. Monteiro Departamento de Química, CCET, Universidade Federal do Maranhão, São Luís, MA, CEP 65085-580, Brazil

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A. G. Souza Departamento de Química, CCEN, Universidade Federal da Paraíba, João Pessoa, PB, CEP 58059-900, Brazil

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L. E. B. Soledade Departamento de Química, CCEN, Universidade Federal da Paraíba, João Pessoa, PB, CEP 58059-900, Brazil

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N. Queiroz Departamento de Química, CCEN, Universidade Federal da Paraíba, João Pessoa, PB, CEP 58059-900, Brazil

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A. L. Souza Departamento de Química, CCEN, Universidade Federal da Paraíba, João Pessoa, PB, CEP 58059-900, Brazil

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V. E. Mouchrek Filho Departamento de Química, CCET, Universidade Federal do Maranhão, São Luís, MA, CEP 65085-580, Brazil

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A. F. F. Vasconcelos Departamento de Química e Biologia, Universidade Estadual do Maranhão, São Luís, MA, CEP 65055-970, Brazil

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Abstract

The vegetal species Pimenta dioica Lindl, popularly known as Jamaican pepper, is a 6–15 m tall tree, which belongs to the Mirtaceae family. Its fruits have an essential oil of great economic value in the international market, due to its high level of eugenol (its major compound), which is largely used in chemical and pharmaceutical industries. In this work, the extraction of the essential oil from the fruits of Pimenta dioica Lindl was carried out by the hydrodistillation method, using a modified Clevenger system. It was observed that the volume of the extracted oil reaches a maximum at 4 h, with a yield of 2.7% (m/m). The essential oil was characterized by physico-chemical analyses, such as density, refraction index, ethanol solubility, color, and appearance, besides UV–vis and infrared spectroscopy and gas chromatography/mass spectrometry. Thus, eugenol was confirmed as the major component of the essential oil of Pimenta dioica Lindl (77%). The technique of differential scanning calorimetry (DSC) was used for the determination of boiling point of the sample of essential oil from the fruits of Pimenta dioica (L.).

  • 1. Seidemann J . Pimenta Lindl.—Allspice—Myrtaceae. In: World spice plants. Heidelberg: Springer-Verlag; 2005. p. 2867.

  • 2. Weyerstahl, P, Weyerstahl, HM, Christiansen, C, Oguntimein, BO, Adeoye, AO. Volatile constituents of Eugenia uniflora leaf oil. Planta Med. 1988;54:546549. .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 3. Oliveira, RA, Reis, TV, Sacramento, CK, Duarte, LP, Oliveira, FF. Volatile chemical constituents of rich spices in eugenol. Braz J Pharmacogn. 2009;19:771775.

    • Search Google Scholar
    • Export Citation
  • 4. Nitta, Y, Kikuzaki, H, Ueno, H. Inhibitory activity of Pimenta dioica extracts and constituents on recombinant human histidine decarboxylase. Food Chem. 2009;113:445449. .

    • Crossref
    • Search Google Scholar
    • Export Citation
  • 5. Jirovetz, L, Buchbauer, G, Stoilova, I, Krastanov, A, Stoyanova, A, Schmidt, E. Spice plants: chemical composition and antioxidant properties of Pimenta Lindl. essential oils, part 1: Pimenta dioica (L.) Merr. leaf oil from Jamaica. Nutrition. 2007;31:5563.

    • Search Google Scholar
    • Export Citation
  • 6. Duke, JA. Handbook of medicinal herbs. Florida: CRC; 1985.

  • 7. Bacis-Boelens Aroma Chemical Information Service: Pimento VCH volatile compounds in food database. Zeist: TNO Nutrition and Food Research; 2000.

    • Search Google Scholar
    • Export Citation
  • 8. Sharma, R. Pimenta. Medicinal plants of India—an encyclopaedia. New Delhi: Data Publishing House Delhi; 2003.

  • 9. Takemasa, M. Allspice. Encyclopedia of spice. Tokyo: Bunensha; 2006.

  • 10. Oussalah, M, Caillet, S, Saucier, L, Lacroix, M. Antimicrobial effects of selected plant essential oils on the growth of four pathogenic bacteria: E. coli O157:H7, Salmonella typhimurium, Staphylococcus aureus and Listeria monocytosenes. Food Control. 2007;18:414420. .

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    • Export Citation
  • 11. Chaar, JS, Mouchreck-Filho, VE, Breviglieri, ST, Cavalheiro, ÉTG, Chierice, GO. Boiling temperatures and enthalpy changes of essential oils using capillary glass sample holder. J Therm Anal Calorim. 2004;75:437443. .

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    • Export Citation
  • 12. Mouchrek Filho VE . Estudos Analíticos e modificações químicas por metilação e acetilação do eugenol contido no óleo essencial extraído das folhas da espécie Pimenta dioica Lindl. São Carlos. Ph.D. Thesis, Instituto de Química de São Carlos, USP, Brazil, 2000.

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  • 13. Silverstein, RM, Webster, FX, Kiemle, DJ. Spectrometric identification of organic compounds. 5 New York: Wiley; 2006.

  • 14. The Merck Index chemistry’s constant companion. 14th ed. Whitehouse Station, NJ, USA: Merck & Co., Inc.; 2006.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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