Geopolymers
Inorganic polymeric new materials
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C. Alosious Gonsago
C. Alosious Gonsago
Department of Physics, A. J. College of Engineering, Chennai 302, India
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Helen Merina Albert
Helen Merina Albert
Department of Physics, Sathyabama University, Chennai 119, India
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P. Malliga
P. Malliga
Department of Physics, Sathyabama University, Chennai 119, India
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A. Joseph Arul Pragasam
A. Joseph Arul Pragasam
Department of Physics, Sathyabama University, Chennai 119, India
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Abstract
A novel nonlinear optical semi-organic single crystal of l-histidine methyl ester dihydrochloride was grown by slow evaporation solution growth method at an ambient temperature. The grown crystal was characterized by single crystal X-ray diffraction. Functional groups and the modes of vibrations were identified by FT–IR spectroscopy. The chemical composition of the crystal was confirmed by Energy dispersive X-ray analysis. The optical behavior of the crystal was examined by UV spectral analysis, which shows the absence of absorption between the wavelengths ranging from 230 to 1000 nm. The optical band gap of the grown crystal was estimated and is found to be 5.35 eV. The thermal behavior of the crystal was investigated by thermogravimetric and differential thermal analyses. The nonlinear optical property of the grown crystal was confirmed by the powder technique of Kurtz and Perry.
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-
1. Rajasekaran, M, Anbusrinivasan, P, Mojumdar, SC. Growth, spectral and thermal characterization of 8-hydroxyquinoline. J Therm Anal Calorim. 2010;100:827–830. .
-
2. Moitra, S, Kar, T. Growth and characterization of l-valine- a nonlinear optical crystal. Cryst Res Technol. 2010;45:70–74. .
-
3. Krishnan, C, Selvarajan, P, Freeda, TH. Growth and studies of pure and lithium bromide-doped zinc tris-thiourea sulfate (ZTS) single crystals. Mater Manufact Process. 2008;23:800–804. .
-
4. Lydia Caroline, M, Kandasamy, A, Mohan, R, Vasudevan, S. Growth and characterization of dichloro bis l-proline Zn(II): a semiorganic nonlinear optical crystal. J Cryst Growth. 2009;311:1161–1165. .
-
5. Senthil, A, Ramasamy, P. Synthesis, growth and characterization of strontium bis (hydrogen l-malate) hexahydrate bulk single crystal: a promising semi-organic nonlinear optical material. J Cryst Growth. 2010;312:276–281. .
-
6. Kandasamy, A, Siddeswaran, R, Murugakoothan, P, Suresh Kumar, P, Mohan, R. Synthesis, growth and characterization of l-proline cadmium chloride monohydrate (L-PCCM) crystals—a new nonlinear optical material. Cryst Growth Design. 2007;7:183–186. .
-
7. Marcy, HO, Rosker, MJ, Warren, LF, Cunningham, PH, Thomas, CA. l-histidine tetrafluoroborate: a solution-grown semiorganic crystal for nonlinear frequency conversion. Opt Lett. 1995;20: 3 252–254. .
-
8. Madhavan, J, Aruna, S, Thomas, PC, Vimalan, M, Rajasekar, SA, Sagayaraj, P. Growth and characterization of l-histidine hydrochloride monohydrate single crystals. Cryst Res Technol. 2007;42:59–64. .
-
9. Ramajothi, J, Danuskodi, S. Crystal growth, thermal and optical studies on a semiorganic nonlinear optical material for blue-green laser generation. Spectrochim Acta A. 2007;68:1213–1219. .
-
10. Madhavan, J, Aruna, S, Praba, K, Julius, JP, Jinson, J, Joseph, P, Selvakumar, S, Sagayaraj, P. Growth and characterization of novel NLO crystal l-histidine hydrofluoride dihydrate (LHHF). J Cryst Growth. 2006;293:409–414. .
-
11. Aruna, S, Vimalan, M, Thomas, PC, Thamizharasan, K, Ambugam, K, Madhavan, J, Sagayaraj, P. Growth and characterization of semi organic nonlinear optical crystals. Cryst Res Technol. 2007;304:180–185. .
-
12. Petrosyan, HA, Karapetyan, HA, Petrosyan, AM. l-Histidine nitrates. J Mol Struct. 2006;794:160–167. .
-
13. Madhavan, J, Aruna, S, Ambujam, K, Pragasam, AJA, Ravikumar, SM, Mohamed, MG, Sagayaraj, P. Crystallization and characterization of nonlinear optical l-histidinium dihydrogen orthophosphate orthophosporic acid single crystal. Cryst Res Technol. 2006;41:997–1001. .
-
14. Jayaraman, R, Sivasubramanian, D. Optical and microhardness studies of semiorganic nonlinear optical material: l-histidine tetrafluoroborate. Cryst Res Technol. 2003;38:986–991. .
-
15. Sun, GH, Sun, XT, Sun, ZH, Wang, XQ, Liu, XJ, Zhang, GH, Xu, D. Growth and characterization of a nonlinear optical crystal: l-histidine trifluoroacetate. J Cryst Growth. 2009;311:3904–3910. .
-
16. Vilchiz, VH, Norman, RE, Chang, SC. l-Histidine methyl ester dihydrochloride. Acta Crystallogr C. 1996;51:696–698. .
-
17. Madhurambal, G, Mariappan, M, Mojumdar, SC. Thermal, UV and FTIR spectral studies of urea–thiourea zinc chloride single crystal. J Therm Anal Calorim. 2010;100:763–768. .
-
18. Madhurambal, G, Ramasamy, P, Anbusrinivasan, P, Vasudevan, G, Kavitha, S, Mojumdar, SC. Growth and characterization studies of 2-bromo-40-chloro-acetophenone (BCAP) crystals. J Therm Anal Calorim. 2008;94:59–62. .
-
19. Parthiban, S, Murali, S, Madhurambal, G, Meenakshisundaram, SP, Mojumdar, SC. Effect of zinc(II) doping on thermal and optical properties of potassium hydrogen phthalate (KHP) crystals. J Therm Anal Calorim. 2010;100:751–756. .
-
20. Ramasamy, G, Parthiban, S, Meenakshisundaram, SP, Mojumdar, SC. Influence of alkali metal sodium doping on the properties of potassium hydrogen phthalate (KHP) crystals. J Therm Anal Calorim. 2010;100:861–865. .
-
21. Muthu, K, Bhagavannarayana, G, Chandrasekaran, C, Parthiban, S, Meenakshisundaram, SP, Mojumdar, SC. Os(VIII) doping effects on the properties and crystalline perfection of potassium hydrogen phthalate (KHP) crystals. J Therm Anal Calorim. 2010;100:793–799. .
-
22. Meenakshisundarm, SP, Parthiban, S, Madhurambal, G, Mojumdar, SC. Effect of chelating agent (1,10-phenanthroline) on potassium hydrogen phthalate crystals. J Therm Anal Calorim. 2008;94:21–25. .
-
23. Mojumdar, SC, Sain, M, Prasad, RC, Sun, L, Venart, JES. Selected thermoanalytical methods and their applications from medicine to construction. J Therm Anal Calorim. 2007;60:653–662. .
-
24. Varshney, G, Agrawal, A, Mojumdar, SC. Pyridine based cerium(IV) phosphate hybrid fibrous ion exchanger: Synthesis, characterization and thermal behaviour. J Therm Anal Calorim. 2007;90:731–734. .
-
25. Madhurambal, G, Ramasamy, P, Anbusrinivasan, P, Mojumdar, SC. Thermal properties, induction period, interfacial energy and nucleation parameters of solution grown benzophenone. J Therm Anal Calorim. 2007;90:673–679. .
-
26. Mojumdar, SC. Thermoanalytical and IR-spectral investigation of Mg(II) complexes with heterocyclic ligands. J Therm Anal Calorim. 2001;64:629–636. .
-
27. Pragasam, AJA, Selvakumar, S, Thamizharasan, K, Anand, DP, Sagayaraj, P. Growth and optical characterization of Cu− and Mg− substituted l-arginine di phosphate single crystals. J Cryst Growth. 2005;280:271–278. .
-
28. Rao, CNR. Chemical application of infrared spectroscopy. 2 New York: Academic Press; 1963.
-
29. Bellamy, LJ. The infrared spectra of complex molecules. 3 New York: Wiley; 1975.
-
30. Herzberg, G. Infrared and Raman spectra of polyatomic molecules. 1 New York: Van Nostrand Reinhold; 1945.
-
31. Krishnakumar, V, Sivakumar, S, Nagalakshmi, R, Bhuvaneswari, S, Rajaboopathi, M. Effect of doping an organic molecule ligand on TGS single crystals. Spectrochim Acta A. 2008;71:480–485. .
-
32. Fochs, PD. The measurement of the energy gap of semiconductors from their diffuse reflection spectra. Proc Phys Soc London. 1956;B69:70–75.
-
33. Aneesh, PM, Krishna, KM, Jayaraj, MK. Hydrothermal synthesis and characterization of undoped and Eu doped ZnGa2O4 nanoparticles. J Electrochem Soc. 2009;156:33–36. .
-
34. Meenakshisundaram, SP, Parthiban, S, Kalavathy, R, Madhurambal, G, Bhagavannarayana, G, Mojumdar, SC. Thermal and optical properties of ZTS single crystals in the presence of 1,10-phenanthroline (Phen). J Therm Anal Calorim. 2010;100:831–837. .
-
35. Kurtz, SK, Perry, TT. A powder technique for the evaluation of non-linear optical materials. J Appl phys. 1968;39:3798–3813. .
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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