Geopolymers
Inorganic polymeric new materials
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Jozef Rychlý
Jozef Rychlý
Polymer Institute, Slovak Academy of Sciences, Dúbravská cesta 11, 84541, Bratislava, Slovakia
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Agnes Lattuati-Derieux
Agnes Lattuati-Derieux
Centre de Recherche sur la Conservation des Collections, Muséum National d’Histoire Naturelle, MCC, CNRS, 36 rue Geoffroy-Saint-Hilaire, 75005, Paris, France
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Lyda Matisová-Rychlá
Lyda Matisová-Rychlá
Polymer Institute, Slovak Academy of Sciences, Dúbravská cesta 11, 84541, Bratislava, Slovakia
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Katarína Csomorová
Katarína Csomorová
Polymer Institute, Slovak Academy of Sciences, Dúbravská cesta 11, 84541, Bratislava, Slovakia
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Ivica Janigová
Ivica Janigová
Polymer Institute, Slovak Academy of Sciences, Dúbravská cesta 11, 84541, Bratislava, Slovakia
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Bertrand Lavédrine
Bertrand Lavédrine
Centre de Recherche sur la Conservation des Collections, Muséum National d’Histoire Naturelle, MCC, CNRS, 36 rue Geoffroy-Saint-Hilaire, 75005, Paris, France
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Abstract
Non-isothermal thermogravimetry, differential scanning calorimetry and chemiluminescence were used for characterization of degradation of pre-aged nitrocellulose in order to elucidate the optimal route of extrapolation of rate constants from the region of the autoaccelerated reaction to lower temperatures. First order rate constants, the one characterizing the decomposition of nitrocellulose in the rate auto-accelerating region and the two constants corresponding to the slow process in induction period of nitrocellulose decomposition were shown to provide a sufficient description. The rate constants determined for several temperatures were shown to depend on the amount of char residue which is formed from pre-aged samples after the thermogravimetry runs from 40 to 550 °C.
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| Journal of Thermal Analysis and Calorimetry | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1969 |
| Volumes per Year |
1 |
| Issues per Year |
24 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1388-6150 (Print) |
| ISSN | 1588-2926 (Online) |
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Temperature dependence of the rate of reaction in thermal analysis
The Arrhenius equation in condensed phase kinetics
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